Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC

ZHA Dao-cheng1; FENG Dong-lan1; LI Lin-xiao2; NIU Lan-ling2

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Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC

更新时间：2024-09-23

- Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 9, Pages: 129-131(2013)
- 作者机构：
  
  1. 南阳医学高等专科学校
  2. 河南华茸堂药业有限公司
- 作者简介：
- 基金信息：
- DOI：
  CLC： R286
- Published：2013
- 稿件说明：
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[1]查道成,冯冬兰,李林晓,牛兰玲.HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量[J].中国实验方剂学杂志,2013,19(09):129-131.

ZHA Dao-cheng1, FENG Dong-lan1, LI Lin-xiao2, et al. Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 129-131.
[1]查道成,冯冬兰,李林晓,牛兰玲.HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量[J].中国实验方剂学杂志,2013,19(09):129-131. DOI：

ZHA Dao-cheng1, FENG Dong-lan1, LI Lin-xiao2, et al. Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 129-131. DOI：

摘要

目的:建立HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱含量测定方法。方法:色谱柱为大连依利特C18（4.6 mm×200 mm

5μm）

以乙腈-0.1%磷酸溶液（含0.1%三乙胺）（3∶97）为流动相

流速1 mL.min-1

检测波长205 nm

柱温30℃。结果:盐酸麻黄碱与样品中其他组分分离效果好

盐酸麻黄碱进样量在0.188～0.940μg具有良好线性关系

平均回收率99.39%

RSD 1.38%（n=6）。结论:方法简便易行

准确可靠

所建的方法可用于冯了性风湿跌打药酒的质量控制。

Abstract

Objective:To establish an HPLC method for determination of ephedrine hydrochloride in Fengliaoxing Fengshi Dieda wine.Method: The chromatographic column was Yilite C18（4.6 mm×200 mm

5 μm）;the mobile phase was acetonitril-0.1% phosphoric acid（0.1% triethameamine）（3∶ 97）;the flow rate was 1 mL · min-1;the detecting wavelength was set at 205 nm

and the column temperature was kept at 30 ℃.Result: The linear range of ephedrine hydrochloride was 0.188-0.940 μg.The average recovery was 99.39% and RSD was 1.38%（n=6）.Conclusion: The method established was accuracy

sensitive and simple.It can be used for quality control of Fengliaoxing Fengshi Dieda wine.

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Related Author

ZHA Dao-cheng

FENG Dong-lan

LI Lin-xiao

NIU Lan-ling

YANG Qing

GUO Yan-rong

CHEN Ying

HUANG Xue-mei

Related Institution

Level 3 Laboratory for State Administration of Traditional Chinese Medicine,Beijing Zhendong Guangming Pharmaceutical Research Institute Co.,Ltd

Institute of Chinese Meteria Medica,China Academy of Chinese Medical Sciences

Department of Pharmacy,Affiliated Hospital of Medical College of Chinese People’s Armed Police Forces

2 Protection and Utilization of Traditional Chinese Medicine of Beijing Area Major Laboratory,Beijing Normal University

Jilin Agricultural University

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