Fingerprinting of Qingfei Yihuo Tablets and its Application in Quality Control

WANG Lin1; GUO Dong-qin2; ZHOU Nong1; XIE Jing3; XU Jing1

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Fingerprinting of Qingfei Yihuo Tablets and its Application in Quality Control

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- Fingerprinting of Qingfei Yihuo Tablets and its Application in Quality Control
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 9, Pages: 114-117(2013)
- 作者机构：
  
  1. 大理学院药学院
  2. 重庆三峡学院生命科学与工程学院
  3. 重庆市食品药品检验所
- 作者简介：
- 基金信息：
- DOI：
  CLC： R286.0
- Published：2013
- 稿件说明：
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[1]王琳,郭冬琴,周浓,谢静,徐静.清肺抑火片指纹图谱的建立及其在质量控制中的应用[J].中国实验方剂学杂志,2013,19(09):114-117.

WANG Lin1, GUO Dong-qin2, ZHOU Nong1, et al. Fingerprinting of Qingfei Yihuo Tablets and its Application in Quality Control[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 114-117.
[1]王琳,郭冬琴,周浓,谢静,徐静.清肺抑火片指纹图谱的建立及其在质量控制中的应用[J].中国实验方剂学杂志,2013,19(09):114-117. DOI：

WANG Lin1, GUO Dong-qin2, ZHOU Nong1, et al. Fingerprinting of Qingfei Yihuo Tablets and its Application in Quality Control[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 114-117. DOI：

摘要

目的:建立清肺抑火片HPLC指纹图谱。方法:采用UltrasphereTM-ODS-C18柱（4.6 mm×250 mm

5μm）

流动相0.1%磷酸溶液（A）-乙腈（B）梯度洗脱

检测波长270 nm

流速1.0 mL.min-1

柱温40℃。结果:不同厂家的清肺抑火片指纹图谱变异范围差异显著

同一厂家的产品质量基本稳定在一定水平内。结论:该方法可用于测定不同来源清肺抑火片的色谱指纹图谱

并为其全面质量评价和生产工艺监控提供了可行的方法。

Abstract

Objective:To establish the HPLC fingerprint of Qingfei Yihuo Tablets.Method: Ultrasphere TM-ODS-C18 column（4.6 mm ×250 mm

5 μm） was used

the mobile phase was 0.1% phosphoric acid solution（A）-acetonitrile（B） gradient elution

the detection wavelength was set at 270 nm.The flow rate was 1 mL ·min-1

and column temperature was kept at 40 ℃.Result: Fingprints of the tablets from different manufacturers varies significantly

which keep stable at a certain level from the same manufacture.Conclusion: The method can be used for the determination of different source of Qingfei Yihuo Tablets and can provide a feasible method for comprehensive quality evaluation and production process monitoring.

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Related Author

WANG Lin

GUO Dong-qin

ZHOU Nong

XIE Jing

XU Jing

FAN Wei-feng

ZHENG Zhao-guang

HU Qin

Related Institution

School of Pharmacy,Chengdu University of Traditional Chinese Medicine ( TCM )

Chengdu Yonkon Pharmacy Co. Ltd.

Teaching Hospital of Chengdu University of TCM

Changzhi Medical College

Shanxi Zhendong Pharmaceutical Co. Ltd.

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