HPLC Assaying of Aconitine in Xiaojin Pills

PING Yu-hui; ZONG Xing-xing; GUAN Zhi-yu; MAO Hong-mei

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HPLC Assaying of Aconitine in Xiaojin Pills

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- HPLC Assaying of Aconitine in Xiaojin Pills
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 9, Pages: 80-82(2013)
- 作者机构：
  
  江西中医学院
- 作者简介：
- 基金信息：
- DOI：
  CLC： R286.0
- Published：2013
- 稿件说明：
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[1]平欲晖,宗星星,关志宇,毛红梅.HPLC测定小金丸中乌头碱的含量[J].中国实验方剂学杂志,2013,19(09):80-82.

PING Yu-hui, ZONG Xing-xing, GUAN Zhi-yu, et al. HPLC Assaying of Aconitine in Xiaojin Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 80-82.
[1]平欲晖,宗星星,关志宇,毛红梅.HPLC测定小金丸中乌头碱的含量[J].中国实验方剂学杂志,2013,19(09):80-82. DOI：

PING Yu-hui, ZONG Xing-xing, GUAN Zhi-yu, et al. HPLC Assaying of Aconitine in Xiaojin Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 80-82. DOI：

摘要

目的:建立高效液相色谱法测定小金丸中乌头碱的含量。方法:采用ultimate C18柱（4.6 mm×250 mm

5μm）

以甲醇-0.03 mol.L-1磷酸二氢钾溶液-三乙胺（45∶55∶0.04）为流动相

流速1.0 mL.min-1

检测波长240 nm

柱温25℃。结果:乌头碱在0.114～2.28μg具有良好的线性关系（r=0.999 8）

平均回收率为97.79%

RSD 2.31%。结论:该方法准确、灵敏

重复性好

可用于小金丸中乌头碱的含量测定。

Abstract

Objective:To establish a HPLC method for the assaying of aconitine in Xiaojin pills.Method: C18（4.6 mm×250 mm

5 μm） was used with methanol-30 mmol · L-1phosphate solution-triethylamine（45∶55∶0.04） as the mobile phase.The flow rate was 1.0 mL · min-1 and the detection wavelength was set at 240 nm.Result: Aconitine concentration presented a good linear range of 0.114-2.28 μg（r=0.999 8）.The average recovery was 97.79% and RSD was 2.31%.Conclusion: This method is rapid

simple

accurate and suitable for the quality control of the pill.

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Related Author

PING Yu-hui

ZONG Xing-xing

GUAN Zhi-yu

MAO Hong-mei

REN Xin-xin

LI Xing-hua

YE Sha

MA Xiao-ya

Related Institution

Beijing Zhongyan Tongrentang Pharmaceutical Research and Development Co. Ltd.

Beijing Tongrentang Science and Technology Development Co. Ltd.

College of Pharmaceutical Science, Yunnan University of Traditional Chinese Medicine

Henan University of Chinese Medicine

Zhongjing Wanxi Pharmaceutical Co. Ltd.

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