Quality Standard for Qingre Jiedu Tablets

FEI Yi-qin; NIE Jing

您当前的位置：

首页 >

文章列表页 >

Quality Standard for Qingre Jiedu Tablets

更新时间：2024-09-23

- Quality Standard for Qingre Jiedu Tablets
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 9, Pages: 92-95(2013)
- 作者机构：
  
  湖北省食品药品监督检验研究院
- 作者简介：
- 基金信息：
- DOI：
  CLC： R286
- Published：2013
- 稿件说明：
移动端阅览
[1]费毅琴,聂晶.清热解毒片质量标准[J].中国实验方剂学杂志,2013,19(09):92-95.

FEI Yi-qin, NIE Jing. Quality Standard for Qingre Jiedu Tablets[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 92-95.
[1]费毅琴,聂晶.清热解毒片质量标准[J].中国实验方剂学杂志,2013,19(09):92-95. DOI：

FEI Yi-qin, NIE Jing. Quality Standard for Qingre Jiedu Tablets[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 92-95. DOI：

摘要

目的:完善提高清热解毒片的质量标准。方法:采用薄层色谱法对方中金银花、玄参、连翘、栀子、麦冬进行定性鉴别;同时采用高效液相色谱法测定方中黄芩苷和栀子苷的含量

色谱柱COSMOSIL C18-MS-Ⅱ（4.6 mm×250 mm

5μm）

流动相甲醇-0.2%磷酸溶液

梯度洗脱

流速1.0 mL.min-1

柱温30℃

检测波长238 nm。结果:薄层色谱鉴别专属性强

重复性好。黄芩苷和栀子苷含量的平均回收率分别为95.4%

99.3%

RSD分别为2.2%

1.7%（n=6）。结论:该法简便、专属、准确

可用于清热解毒片的质量控制。

Abstract

Objective:To improve the quality for Qingre Jiedu Tablets.Method: Lonicerae Japonicae Flos

Scrophulariae Radix

Forsythiae Fructus

Gardeniae Fructus

Ophiopogonis Radix were indentified by TLC.The content of baicalin and geniposide were determined by HPLC.Cosmosil C18-MS-Ⅱ column was used with the mobile phase of methanol-0.2% phosphatic acid in a gradient manner.The detection wavelength was set up at 238 nm.The flow rate was 1.0 mL · min-1and the column temperature was set at 30 ℃.Result: The average recovery was 95.4% with RSD 2.2% for baicalin

99.3% with RSD 1.7% for geniposide（n=6）.Conclusion: The method is simple

exclusive and accurate

which can be used for determination and quality control for Qingrejiedu Tablets.

关键词

Keywords

references

Views

148

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Quality Standard for Qingre Jiedu Tablets

Studies on Qualitative and Quantitative Methods of Liangge Pills

Studies on the Quality standard of Bimintong Capsule

Quality Standard Study for Kangan Liyan Capsule

Study on the Quality Standard of Licorice Juice as A Processing Excipient

Related Author

FEI Yi-qin

NIE Jing

SHI Tao1

MENG Xian-sheng2

LUO Guo-an2

WANG Yi-ming2

Related Institution

Gansu Province Hospital of Traditional Chinese Medicine

Acupuncture and Moxibustion Hospital Affiliated to Anhui College of Traditional Chinese Medicine & Anhui Modern Engineering Technology Research Center of Chinese Medicine

Shanxi Renyuantang Pharmaceutical Co.,Ltd.

Shanxi University of Traditional Chinese Medicine

Natural Pharmaceutical R&D

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰