GC-MS Analysis of Volatile Oil from Barks of Juglans mandshurica by Different Extraction Methods

LI Jin-feng1; SHI Bo2; DU Rui-juan1; SUN Zhi1; HOU Xiao-hong1

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GC-MS Analysis of Volatile Oil from Barks of Juglans mandshurica by Different Extraction Methods

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- GC-MS Analysis of Volatile Oil from Barks of Juglans mandshurica by Different Extraction Methods
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 9, Pages: 62-65(2013)
- 作者机构：
  
  1. 沈阳药科大学制药工程学院
  2. 沈阳市喷漆工具厂
- 作者简介：
- 基金信息：
- DOI：
  CLC： R284
- Published：2013
- 稿件说明：
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[1]李金凤,施勃,杜瑞娟,孙志,侯晓虹.不同方法提取核桃楸皮挥发油的气质联用分析[J].中国实验方剂学杂志,2013,19(09):62-65.

LI Jin-feng1, SHI Bo2, DU Rui-juan1, et al. GC-MS Analysis of Volatile Oil from Barks of Juglans mandshurica by Different Extraction Methods[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 62-65.
[1]李金凤,施勃,杜瑞娟,孙志,侯晓虹.不同方法提取核桃楸皮挥发油的气质联用分析[J].中国实验方剂学杂志,2013,19(09):62-65. DOI：

LI Jin-feng1, SHI Bo2, DU Rui-juan1, et al. GC-MS Analysis of Volatile Oil from Barks of Juglans mandshurica by Different Extraction Methods[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 62-65. DOI：

摘要

目的:分析核桃楸皮挥发油的主要化学成分。方法:分别采用汽汽萃取法和水蒸气蒸馏法提取核桃楸皮中挥发油

并通过GC-MS技术对其化学成分进行分析

面积归一化法计算各成分的相对百分含量。结果:汽汽萃取法提取的挥发油共鉴定出34种成分

占挥发油总成分97.76%;水蒸气蒸馏法提取的挥发油共鉴定出19种成分

占挥发油总成分69.06%。结论:两种提取方法得到的核桃楸皮挥发油组分与含量差别较大

为全面了解核桃楸皮中挥发性成分及其进一步开发应用提供了实验依据。

Abstract

Objective:To analyze the main chemical constituents of volatile oil from barks of Juglans mandshurica.Method:Volatile oil from barks of Juglans mandshurica was extracted by vapour-vapour extraction method（VVE） and steam distillation method（SD）

respectively.These constituents separated from the volatile oil were identified by GC-MS

and the relative percentage of these constituents were calculated by area normalization method.Result:34 components in volatile oil extracted by VVE were separated and identified

which took 97.76% of the total volatile oil;19 constituents in volatile oil extracted by SD were also separated and identified

and their relative percentage was 69.06% of the total volatile oil.Conclusion:The constituents and content of volatile oil extracted by VVE and SD exhibited significant differences

these results provided experimental basis for understanding the constituents and further exploitation of volatile oil from barks of J.mandshurica.

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Related Author

LI Jin-feng

SHI Bo

DU Rui-juan

SUN Zhi

HOU Xiao-hong

XU Wen-hui

LIANG Qian

LIU Jiang-hua

Related Institution

Key Laboratory for Forest Resources Conservation and Utilization in Southwest Mountains of China, Ministry of Education,Southwest Forestry University

State Key Laboratory of Southwestern Chinese Medicine Resources， Chengdu University of Traditional Chinese Medicine

Basic Medical College， Heilongjiang University of Chinese Medicine

College of Pharmacy， Heilongjiang University of Chinese Medicine

Hubei Research Center of Chinese Materia Medica Processing Engineering and Technology， School of Pharmacy，Hubei University of Chinese Medicine

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