Determination of Mulberroside A in  by HPLC

FANG Jing; GAO Fei; WU Hong-wei; LI Shao-jing; XU Hai-yu; YANG Hong-jun; YANG Lan; FU Mei-hong; LIU Feng

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Determination of Mulberroside A in by HPLC

更新时间：2024-09-23

- Determination of Mulberroside A in by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 5, Pages: 80-82(2013)
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- Published：2013
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FANG Jing, GAO Fei, WU Hong-wei, et al. Determination of Mulberroside A in by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 80-82.
DOI：

FANG Jing, GAO Fei, WU Hong-wei, et al. Determination of Mulberroside A in by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 80-82. DOI：

摘要

目的: 建立桑枝中桑皮苷A的含量测定方法。方法: Dikma Diamonsil C18色谱柱(4.6 mm×250 mm

5 μm)

流动相为甲醇-水(15∶85)

检测波长324 nm

柱温30 ℃

流速1 mL·min-1。结果: 桑皮苷A在10.34~206.8 μg呈良好线性关系(r=0.999 9)

平均回收率99.8%;11批桑枝药材中桑皮苷A含量在0.10%~1.69%。结论: 此法准确、简便、快速

可用于检测桑枝中桑皮苷A的含量。

Abstract

Objective:To establish a method for the determination of mulberroside A in Ramulus Mori by HPLC. Method: Dikma Diamonsil C18 column (4.6 mm×250 mm

5 μm) was used. The mobile phase consisted of methanol and water (15∶85). The temperature of column was maintained at 30 ℃. The flow rate was 1.0 mL·min-1 and the detection wavelength was set at 324 nm. Result: The calibration curve was in good linearity within the range from 10.34 to 206.8μg (r=0.999 9). The average recovery was 99.8%. The content of mulberroside A in Ramulus Mori in defferent areas was 0.10%-1.69%. Conclusion: The method is simple

rapid as well as precise and reliable

and can be used for the determination of mulberroside A in Ramulus Mori.

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Related Author

FANG Jing1

GAO Fei2

WU Hong-wei1

LI Shao-jing1

XU Hai-yu1

YANG Hong-jun1

YANG Lan1

FU Mei-hong1

Related Institution

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

School of Traditional Chinese Medicine,Capital Medical University

Shanxi Buchang Pharmaceutical Co.Ltd

School of Pharmaceutical Sciences， Changchun University of Chinese Medicine

Jilin Ginseng Academy，Changchun University of Chinese Medicine

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