Study on Quality Standard of Anti-inflammation Pills

YU Hong-yan; XU Cheng-gang; LIU Wei; CUI Yong-xia

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Study on Quality Standard of Anti-inflammation Pills

更新时间：2024-01-04

- Study on Quality Standard of Anti-inflammation Pills
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 6, Pages: 164-166(2013)
- 作者机构：
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- Published：2013
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YU Hong-yan, XU Cheng-gang, LIU Wei, et al. Study on Quality Standard of Anti-inflammation Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(6): 164-166.
DOI：

YU Hong-yan, XU Cheng-gang, LIU Wei, et al. Study on Quality Standard of Anti-inflammation Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(6): 164-166. DOI：

摘要

目的: 建立抗炎消肿丸的质量标准。方法: 采用薄层色谱法(TLC)鉴别成方制剂中地丁、蒲公英、栀子、连翘

以HPLC测定黄芩苷的含量。结果: TLC鉴别可明显鉴别地丁、蒲公英、栀子、连翘

黄芩苷在0.016 48～0.082 4 g·L-1线性关系良好(r=1)

平均回收率为99.95%

RSD 0.89%。结论: 该方法操作简便

结果准确

重复性好

可用于该制剂的质量控制。

Abstract

Objective: To establish the quality standard for anti-inflammation pills. Method: Viola yedoensis

Taraxacum mongolicum

Gardenia jasminoides and Forsythia suspense were identified by TLC.Baicalin was determined by HPLC. Result: The results of TLC showed that the relevant spots were clear without interference in the blank reference.The content of baicalin showed a good linearity in the range of 0.016 48-0.082 4 g·L-1 (r=1.0).The average recovery rate was 99.95% and RSD was 0.89%. Conclusion: The established qualitative and quantitative methods are simple

accurate

reliable and reproducible

and can be effectively used for the quality control of anti-inflammation pills.

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Related Author

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CHEN Xin-fa2

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Related Institution

Hubei Institute for Food and Drug Control

Gansu Province Hospital of Traditional Chinese Medicine

齐齐哈尔医学院

齐齐哈尔中医院

黑龙江中医药大学

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