Quality Standard of Xielong Liquor

WANG Ya-zhou; Yang Chun-xu

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Quality Standard of Xielong Liquor

更新时间：2024-01-04

- Quality Standard of Xielong Liquor
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 23, Pages: 105-108(2012)
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- Published：2012
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WANG Ya-zhou, Yang Chun-xu. Quality Standard of Xielong Liquor[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(23): 105-108.
DOI：

WANG Ya-zhou, Yang Chun-xu. Quality Standard of Xielong Liquor[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(23): 105-108. DOI：

摘要

目的: 建立蝎龙酒新的质量标准。方法: 采用薄层色谱法(TLC)定性鉴别处方中的白芍、红花和当归;采用高效液相色谱法对芍药苷、羟基红花黄色素A和阿魏酸进行含量测定。用Inertsil C8-3柱

乙腈-0.1%磷酸-四氢呋喃(18∶80∶2)为流动相

流速1.0 mL·min-1

检测波长340 nm。结果: TLC特征斑点明显、专属性强。芍药苷、羟基红花黄色素A和阿魏酸的线性范围分别为23.35~373.56

5.57~89.08

2.42~38.72 mg·L-1;平均加样回收率分别为101.08%

99.85%

100.34%(n=6)。结论: 所建的新标准可用于蝎龙酒的质量控制。

Abstract

Objective: To study a new quality standard of Xielong liquor. Method: Radix paeoniae alba

flos carthami and radix angelicae sinensis in the the formula were identified qualititively by TLC.The content of paeoniflorin

hydroxysafflor yellow A and ferulic acid was determined by HPLC with a Inertsil C8-3 column. The mobile phase was acetonitrile-0.1% phosphoric acid-tetrahydrofuran(18∶80∶2) with a flow rate at 1.0 mL·min-1.Detection wavelength was at 340 nm. Result: The TLC spots were clear and specific. The linear ranges for paeoniflorin

hydroxysafflor yellow A and ferulic acid were 23.35-373.56

5.57-89.08

2.42-38.72 mg·L-1 respectively. The average recoveries were 101.08%

99.85%

100.34%(n=6). Conclusion: The new established standard can be used for the quality control of Xielong liquor.

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Related Institution

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