HPLC Fingerprint of

LIN Li-mei; LI Chun; LIU Ta-si; XU Zhao-dong; LIU Ju-yan; LIAO Duan-fang

您当前的位置：

首页 >

文章列表页 >

HPLC Fingerprint of

更新时间：2024-01-04

- HPLC Fingerprint of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 22, Pages: 120-123(2012)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Published：2012
- 稿件说明：
移动端阅览
LIN Li-mei, LI Chun, LIU Ta-si, et al. HPLC Fingerprint of [J]. Chinese journal of experimental traditional medical formulae, 2012, 18(22): 120-123.
DOI：

LIN Li-mei, LI Chun, LIU Ta-si, et al. HPLC Fingerprint of [J]. Chinese journal of experimental traditional medical formulae, 2012, 18(22): 120-123. DOI：

摘要

目的: 建立野菊花药材的指纹图谱

为野菊花药材的质量控制提供依据。方法: 采用HPLC

Agilent Eclipse XDB-C18(4.6 mm×250 mm

5 μm)色谱柱

以乙腈-1.0%醋酸水为流动相梯度洗脱

流速1.0 mL·min-1

检测波长290 nm

柱温30 ℃

进样10 μL。结果: 建立了16批野菊花药材的指纹图谱

选择11个野菊花样品作为标准药材

标准药材有16个共有峰

多数峰可以达到较好分离

具有较高的相似度。结论: 建立的高效液相指纹图谱有较好的精密度、重复性和稳定性

可作为野菊花质量评价参考。

Abstract

Objective:To establish HPLC fingerprint of C. indicum to provide the basis for the standards of quality control and identification of the Chinese crude drug. Method: The HPLC method was used on an Agilent Eclipse XDB-C18 (4.6 mm×250 mm

5 μm) column with acetonitrile-0.1% acetic acid as mobile phase by gradient elution at the detection wavelength of 290 nm and the column temperature was set at 30 ℃ with the flow rate of 1.0 mL·min-1; the sample injection was 10 μL. Result: HPLC fingerprints of 16 samples of C. indicum were established. 16 common peaks were selected as the fingerprint peaks in 11 samples. Among the obtained fingerprints

most of the detected peaks were separated effectively. 11 samples had high similarities. Conclusion: The established HPLC fingerprint has desirable accuracy

repeatability and stability

which can be used for one of the quality control of C. indicum.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Study on HPLC Fingerprint of

Discussion on Technical Characteristics of National Drug Standards for Traditional Chinese Medicine Dispensing Granules

Analysis on Quality Standard of Sennae Folium（Cassia angustifolia） Dispensing Granules Based on Standard Decoctions

Herbal Textual Research and Modern Research Progress of Ostreae Concha

Aanlysis on Quality Attribute Transfer Law of Liquid-solid Preparation of Shengxuebao

Related Author

YAO Jiang-xiong

LIAO Duan-fang

HE Ying-chun

LIN Li-mei

CHEN Shengjun

LI Song

GUO Kejia

ZHANG Yuntian

Related Institution

Jiangyin Tianjiang Pharmaceutical Co. Ltd.，Jiangyin

Shandong Technical Innovation Center for Traditional Chinese Medicine Treatment of Respiratory Diseases，Shandong Hongjitang Pharmaceutical Group Co. Ltd.

Shandong Institute for Food and Drug Control

School of Pharmacy，State Key Laboratory of Southwestern Chinese Medicine Resources， Chengdu University of Traditional Chinese Medicine

Hunan Polytechnic of Environment and Biology

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰