Simultaneous Determination of Hydroxysafflor Yellow A and Ferulic Acid in Xielongjiegu Powder by HPLC

WANG Ya-zhou; Yang Chun-xu

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Simultaneous Determination of Hydroxysafflor Yellow A and Ferulic Acid in Xielongjiegu Powder by HPLC

更新时间：2024-01-04

- Simultaneous Determination of Hydroxysafflor Yellow A and Ferulic Acid in Xielongjiegu Powder by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 22, Pages: 109-111(2012)
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- Published：2012
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WANG Ya-zhou, Yang Chun-xu. Simultaneous Determination of Hydroxysafflor Yellow A and Ferulic Acid in Xielongjiegu Powder by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(22): 109-111.
DOI：

WANG Ya-zhou, Yang Chun-xu. Simultaneous Determination of Hydroxysafflor Yellow A and Ferulic Acid in Xielongjiegu Powder by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(22): 109-111. DOI：

摘要

目的: 建立蝎龙接骨散中羟基红花黄色素A和阿魏酸的测定方法。方法: 采用反相高效液相色谱法法进行定量分析

用Inertsil C8-3柱

乙腈-0.2%磷酸-四氢呋喃(28∶70∶2)为流动相

流速1.0 mL·min-1

检测波长340 nm。结果: 羟基红花黄色素A和阿魏酸的线性范围分别为11.13~111.35 mg·L-1和3.42~34.2 mg·L-1;平均加样回收率分别为100.35%

99.23%。结论: 此法简便、准确

具有良好的重复性和回收率

适用于蝎龙接骨散中羟基红花黄色素A和阿魏酸的同时测定。

Abstract

Objective:To establish a method for determination of the content of hydroxysafflor yellow A and ferulic acid in Xielongjiegu powder. Method: The quantitative analysis was carried out by HPLC with a Inertsil C8-3 column. The mobile phase was acetonitrile-0.2% phosphoric acid-tetrahydrofuran(28∶70∶2) with a flow rate at 1.0 mL·min-1.Detection wavelength was set at 340 nm. Result: The linear ranges for hydroxysafflor yellow A and ferulic acid were 11.13-111.35 mg·L-1 and 3.42-34.2 mg·L-1respectively. The average recoveries were 100.35% and 99.23%. Conclusion: This method is simple and accurate with good repeatability and recovery. It is suitable for the determination of the content of hydroxysafflor yellow A and ferulic acid in Xielongjiegu powder.

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