Determination of Paeoniflorin in Qianlie Antong Capsule by HPLC

DING Shi-qiang

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Determination of Paeoniflorin in Qianlie Antong Capsule by HPLC

更新时间：2024-01-04

- Determination of Paeoniflorin in Qianlie Antong Capsule by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 23, Pages: 61-63(2012)
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- Published：2012
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DING Shi-qiang. Determination of Paeoniflorin in Qianlie Antong Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(23): 61-63.
DOI：

DING Shi-qiang. Determination of Paeoniflorin in Qianlie Antong Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(23): 61-63. DOI：

摘要

目的: 采用高效液相色谱建立前列安通胶囊中芍药苷含量的检测方法。方法: 采用Waters Nova-Pak C18色谱柱(4.6 mm×150 mm

4 μm)

以乙腈-水(15∶85)为流动相

流速为1.0 mL·min-1

检测波长230 nm

芍药苷的保留时间为3.757 min。结果: 芍药苷质量在0.20~4.0 μg呈良好线性关系 (r=0.997 6)。低、中、高3 个浓度的平均加样回收率分别为97.85%~100.38% (RSD 0.37%~0.81%)。结论: 该方法简便快速

结果准确可靠

可用于前列安通胶囊中芍药苷的HPLC含量测定。

Abstract

Objective: To determine the content of the paeoniflorin in Qianlie Antong capsule by HPLC. Method: The separation was performed on Waters Nova-Pak C18 (4.6 mm×150 mm

4 μm)column eluted with the mobile phase consisting of acetonitrile-water (15∶85) at the flow rate of 1mL·min-1.The detection wavelength was at 230 nm and the retention time of paeoniforin was 3.757 min. Result: Paeoniflorin showed good linearity(r=0.997 6)in the range of 0.20-4.0 μg.The mean recoveries of low

middle and high concentration of the components were among 97.85%-100.38% (RSD 0.37%-0.81%). Conclusion: The method is rapid

simple

accurate and reliable

and it can be used for determining paeoniflorin in Qianlie Antong capsule.

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