GC-MS Analysis on Liposoluble Components of

LUAN Yang; ZHANG Hui; KANG Ting-guo

您当前的位置：

首页 >

文章列表页 >

GC-MS Analysis on Liposoluble Components of

更新时间：2024-01-04

- GC-MS Analysis on Liposoluble Components of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 2, Pages: 52-54(2013)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Published：2013
- 稿件说明：
移动端阅览
LUAN Yang, ZHANG Hui, KANG Ting-guo. GC-MS Analysis on Liposoluble Components of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(2): 52-54.
DOI：

LUAN Yang, ZHANG Hui, KANG Ting-guo. GC-MS Analysis on Liposoluble Components of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(2): 52-54. DOI：

摘要

目的: 分析掌叶半夏脂溶性成分的化学成分。方法: 对乙醇提取后氯仿萃取得到的脂溶性成分进行了GC-MS分析。HP-5MS色谱柱(0.25 mm×0.25 mm×30 m);程序升温

进样口温度280℃

进样量1.0 μL

分流比10:1。结果: 共分离鉴定出三氯乙酸1.86%

顺式-1

2-环己二醇3.56%

庚基氢过氧化物1.66%

Z型-2-十一碳烯5.54%

1-丁氧基-2-乙基己烯4.13%

吡咯并吡嗪-1

4-二酮6.36%

棕榈酸23.32%

10-十一碳炔酸33.81%

环戊烷十一酸1.11%

5-哌嗪

3-苄基-6-异丙基2.95%

2-溴(正)壬烷1.04%

吡咯并吡嗪-1

4-二酮

六氢-3(苯)5.73%

4-乙基四氢-2H-噻喃1.77%

2溴二十二烷1.26%

1-二氯-2

3-四甲基环丙烷 2.31%

Z)-6

12-十八三烯苯基甲基酯等19种成分。结论: 进一步确定了掌叶半夏脂溶性部分的化学成分

为掌叶半夏的抗肿瘤作用深入研究提供参考。

Abstract

Objective: To analyze the liposoluble components of Pinellia pedatisecta. Method: The liposoluble components of P. pedatisecta were extracted by ethanol; the extract was abstracted by chloroform

which can get liposoluble components and analyzed by gas chromatography-mass spectrometry(GC-MS). Result: Nineteen liposoluble components were identified as trichloroacetic acid 1.86%

cis-1

2-cyclohexanediol 3.56%

heptylhydroperoxide 1.66%

(Z)-2-undecene 5.54%

1-hexene

1-butoxy-2-ethyl-4.13%

pyrrolo pyrazine-1

4-dione

hexahydro-3-(2-methylpropyl)-6.36%

n-hexadecanoic acid 23.32%

10-undecynoic acid 33.81%

cyclopentane undecanoic acid 1.11%

5-piperazinedione

3-benzyl-6-isopropyl-2.95%

2-bromononane 1.04%

pyrrolo pyrazine-1

4-dione

hexahydro-3-(phenylmethy)-5.73%

4-ethyltetrahydro-2H-thiopyran 1.77%

docosane

22-dibromo- 1.26%

cyclopropane

1-dichloro-2

3-tetramethyl- 2.31%

12-octadecatrienoic acid

phenylmethyl ester

Z)1.00%. Conclusion: The liposoluble components of P. pedatisecta have been further determined to establish the basis for antitumous effect.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Age Discrimination Based on Volatile Components of Arisaema Cum Bile

Supercritical CO₂ Extraction of Volatile Oil in Pine Needle of Pinus yunnanensis from Different Habitats and Analysis by GC-MS

Comparison of Volatile Oil of Domestic and Foreign Panacix Quinquefolii Radix by HS-SPME/GC-MS

Study on Volatile Components and Antimicrobial Activities of the Essential Oil from the Leaf of var. major in Daba Mountain

Gas Chromatography-Mass Spectrometry Analysis for Volatile Compounds in by Headspace Injection

Related Author

YUAN Yuan

JIN Yan

LIU Ying

ZHAO Yuyang

LIU Tianrui

NAN Tiegui

HE Jia

YANG Xiao-fang

Related Institution

School of Traditional Chinese Medicine（TCM）， Guangdong Pharmaceutical University

State Key Laboratory for Quality Ensurance and Sustainable Use of Dao-di Herbs， National Resource Center for Chinese Materia Medica， China Academy of Chinese Medical Sciences

Institute of TCM Health Industry，China Academy of Chinese Medical Sciences

Beijing Shuangqiao Yanjing Chinese Medicine Pieces Factory

College of Pharmacy and Chemistry， Dali University， Dali

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰