TLC Identification and HPLC Assay on Trichosanthis Semen

CHAO Zhi-mao; TANG Chun-feng; ZHANG Gui-feng; SUN Wen

您当前的位置：

首页 >

文章列表页 >

TLC Identification and HPLC Assay on Trichosanthis Semen

更新时间：2024-01-04

- TLC Identification and HPLC Assay on Trichosanthis Semen
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 17, Pages: 86-88(2012)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Published：2012
- 稿件说明：
移动端阅览
CHAO Zhi-mao, TANG Chun-feng, ZHANG Gui-feng, et al. TLC Identification and HPLC Assay on Trichosanthis Semen[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(17): 86-88.
DOI：

CHAO Zhi-mao, TANG Chun-feng, ZHANG Gui-feng, et al. TLC Identification and HPLC Assay on Trichosanthis Semen[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(17): 86-88. DOI：

摘要

目的: 建立常用中药瓜蒌子的定性定量方法。方法: 以栝楼仁二醇和α-菠菜甾醇为对照品

建立瓜蒌子的薄层色谱(TLC)鉴别技术;以栝楼仁二醇为对照品

建立高效液相色谱(HPLC)-紫外(PAD)检测的含量测定技术。结果: 12份瓜蒌子的不皂化物

均可显示栝楼仁二醇和α-菠菜甾醇的薄层斑点;瓜蒌子中栝楼仁二醇的含量介于0.056 88%~0.087 28%。结论: 栝楼仁二醇作为瓜蒌子的有效成分

可以作为瓜蒌子质量标准的一个重要指标。建议中药瓜蒌子中栝楼仁二醇的含量不得低于0.05%。

Abstract

Objective: To establish the methods of qualitation and quantitation about Trichosanthis Semen

one of the commonly used Chinese material medica. Method: The thin-layer chromatography (TLC) method was found with the reference substance both karounidiol and α-spinasterol. The HPLC method was found with the PAD and the reference substance of karounidiol. Result: The unsaponifiable matter from all 12 Trichosanthis Semen samples showed the spots of both karounidiol and α-spinasterol on a TLC plate. The content of karounidiol in all 12 Trichosanthis Semen samples was 0.056 88%-0.087 28%. Conclusion: Karounidiol

one of the active components of Trichosanthis Semen

can be considered as an important index of the quality standard of Trichosanthis Semen. The content of karounidiol was suggested not less than 0.05% in Trichosanthis Semen.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Study on Quality Standard of Zhifukang Capsule

Studies on Qualitative and Quantitative Methods of Liangge Pills

Influence of dfferent producing area on quality of Venenum bufonis

Studies on the Quality standard of Bimintong Capsule

Chromatographic Corresponding Identifications in Different Botanical Origins of Sinapis Semen

Related Author

LI Man-ling

FENG Wei-hong

SHI Tao1

MENG Xian-sheng2

LUO Guo-an2

WANG Yi-ming2

Related Institution

Hubei Institute for Food and Drug Control

Natural Pharmaceutical R&D

修正药业长春高新制药有限公司

吉林省中医药科学院

吉林天药本草堂制药有限公司

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰