Determination of Hesperidin in Sucking Tablets of Jinguo by High Performance Capillary Electrophoresis

HUO Tian-feng

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Determination of Hesperidin in Sucking Tablets of Jinguo by High Performance Capillary Electrophoresis

更新时间：2024-01-04

- Determination of Hesperidin in Sucking Tablets of Jinguo by High Performance Capillary Electrophoresis
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 12, Pages: 117-119(2012)
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- Published：2012
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HUO Tian-feng. Determination of Hesperidin in Sucking Tablets of Jinguo by High Performance Capillary Electrophoresis[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(12): 117-119.
DOI：

HUO Tian-feng. Determination of Hesperidin in Sucking Tablets of Jinguo by High Performance Capillary Electrophoresis[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(12): 117-119. DOI：

摘要

目的: 建立金果含片中橙皮苷的高效毛细管电泳测定方法。方法: 以25 mmol·L-1 硼砂缓冲溶液(pH 10.0)为运行缓冲液。分离电压20 kV

压力进样0.5 psi×10 s

柱温25 ℃

检测波长283 nm。结果: 橙皮苷在0.023 8~0.142 9 g·L-1(r=0.999 8)具有良好的线性关系

平均加样回收率为99.57%

RSD 1.0 3%。结论: 方法操作简便、灵敏、快速

适用于金果含片中橙皮苷的质量控制。

Abstract

Objective: To establish high performance capillary electrophoresis(HPCE) method to determine the content of hesperidin in sucking tablets of jinguo. Method: The running buffe consisted of 25 mmol·L-1borax solution(pH 10.0)

applied voltage was 20 kV

injection pressure was 0.5 psi

injection time was 10 s.The chromatogram was detected at 283 nm. The column temperature was 25 ℃. Result: The linear ranges of the hesperidin was 0.023 8-0.142 9 g·L-1(r=0.999 8).Their respective average recovery was 99.57%(RSD 1.03%). Conclusion: The method is simple

sensitive and rapid

it could be used for the quality control of hesperidin in sucking tablets of jinguo.

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Related Institution

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