Optimization of Purification Process for Total Flavonoids from by Macroporous Adsorption Resin
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Optimization of Purification Process for Total Flavonoids from by Macroporous Adsorption Resin
Chinese Journal of Experimental Traditional Medical FormulaeVol. 18, Issue 11, Pages: 24-27(2012)
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Published:2012
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LV Zi-ming, Chen Kai, YU Xiang-hong, et al. Optimization of Purification Process for Total Flavonoids from by Macroporous Adsorption Resin[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(11): 24-27.
DOI:
LV Zi-ming, Chen Kai, YU Xiang-hong, et al. Optimization of Purification Process for Total Flavonoids from by Macroporous Adsorption Resin[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(11): 24-27.DOI:
Optimization of Purification Process for Total Flavonoids from by Macroporous Adsorption Resin
Objective: To optimize separation and purification technology of total flavonoids from Glycyrrhiza uralensis by macroporous adsorption resin. Method: Twelve different types of resin were selected with the amount of absorption and desorption ratio of total flavonoids as indexes
based on this
separation and purification technology of total flavonoids were optimized. Result: Purification effect of AB-8 type macroporous was the best
its optimum technology conditions were:the concentration of sample solution 0.2 g·mL-1
maximum sample quantity 2 mL to 1 mL resin
velocity of absorption 0.5 BV·h-1
pH of sample solution 6
6 BV water to remove impurities at 1 BV·h-1
eluted by 4 BV 70% ethanol at flow rate of 1 BV·h-1.Under this optimized process
purity of total alkaloids in elution was 38%. Conclusion: This optimized process was rational
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Purification of Total Flavones from by Macroporous Resins
Purification Process of Total Flavonoids from with Macroporous Resins
Purification Processes of Extract of Scutellaria and Gardenia from Sanhuang Spray with Macroporous Adsorption Resin
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QIU Hong-cong
LIU Bu-ming
SUN Cui
Ru YANG
Cong-yan LIU
Ting XU
Rui-yun LI
Yan CHEN
Related Institution
Affiliated Hospital of Integrated Traditional Chinese and Western Medicine, Nanjing University of Chinese Medicine
Multi-component of Traditional Chinese Medicine (TCM) and Microecology Research Center, Jiangsu Province Academy of TCM
Key Unit of Exploring Effective Substances of Classical and Famous Prescription,State Administration of Traditional Chinese Medicine of the People’s Republic of China
Beijing University of Chinese Medicine
Southen University Key Lab of Traditional Chinese Medicine and New Drug,Guangdong Provincial Key Lab of Traditional Chinese Medicine