Quality Standard of Rukang Capsule

YE Yan-cheng; ZHAO Liang-cun

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Quality Standard of Rukang Capsule

更新时间：2024-01-04

- Quality Standard of Rukang Capsule
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 13, Pages: 125-128(2012)
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- Published：2012
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YE Yan-cheng, ZHAO Liang-cun. Quality Standard of Rukang Capsule[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(13): 125-128.
DOI：

YE Yan-cheng, ZHAO Liang-cun. Quality Standard of Rukang Capsule[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(13): 125-128. DOI：

摘要

目的: 建立乳康胶囊的质量控制方法。方法: 对乳康胶囊中青皮、柴胡进行薄层色谱鉴别;采用HPLC对柴胡皂苷a、柴胡皂苷d进行总含量测定。结果: 薄层色谱斑点清晰

阴性对照无干扰;柴胡皂苷a进样量在2.04~14.28 μg(r=0.999 8)、柴胡皂苷d进样量在2.52-17.64 μg(r=0.9995)线性关系良好。平均回收率为99.15%

RSD 0.54%(n=9)。结论: 建立的TLC和HPLC专属性强、准确度高、重复性好

可用于乳康胶囊的质量控制。

Abstract

Objective: To established the method for quality control of Rukang capsule. Method: Citri Reticulatae Pericarpium viride

Bupleuri Radix in Rukang capsule were identified by TLC.The content of saikosaponin a and Saikosaponin d in Rukang Capsule was determined by HPLC. Result: The spots on the TLC plate were clear and the negative control sample didn't disturb.A good linearity was obtained for saikosaponin a in the range of 2.04-14.28 μg(r=0.9998)and saikosaponin d in the range of 2.52-17.64 μg(r=0.9995).The average recovery was 99.15%(RSD 0.54%

n=9). Conclusion: The method are specific

accurate and reproducible

and can be used for quality control of Rukang capsule.

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Related Author

Yao-hui YE

Yi SHI

Bo-wen ZHANG

Wen-bin CHEN

Ya-nan MA

Huan YU

JIANG Zhen-ou1

LIU Zhi-sheng1

Related Institution

Jiangxi University of Traditional Chinese Medicine

Taiyuan Institute for Food and Drug Control,Taiyan

Shanxi Pharmaceutical Occupational College,Taiyan

Shanxi Shuangren Pharmaceutical Co.Ltd

School of Life Science and Engineering,Southwest Jiaotong University

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