Optimization of Extraction Technology for Fufang Sihuang Suppository

HUANG Bin; HUANG Song; WANG Jie; ZHU De-quan; WANG Pei-pei; LAI Xiao-ping

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Optimization of Extraction Technology for Fufang Sihuang Suppository

更新时间：2024-01-04

- Optimization of Extraction Technology for Fufang Sihuang Suppository
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 3, Pages: 23-25(2012)
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- Published：2012
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HUANG Bin, HUANG Song, WANG Jie, et al. Optimization of Extraction Technology for Fufang Sihuang Suppository[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(3): 23-25.
DOI：

HUANG Bin, HUANG Song, WANG Jie, et al. Optimization of Extraction Technology for Fufang Sihuang Suppository[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(3): 23-25. DOI：

摘要

目的: 优选复方四黄栓的提取工艺。方法: 为提高有效成分的提取率

工艺分为醇提组Ⅰ与醇提组Ⅱ

同时采用单因素结合正交设计法

优选出70%乙醇为提取溶媒

醇提组Ⅰ以盐酸小檗碱含量为指标

醇提组Ⅱ以黄芩苷的含量为指标

优选提取工艺。结果: 醇提组Ⅰ中最佳工艺为70%乙醇共提取3次

每次1.0 h

溶媒倍量为8

6 倍。醇提组Ⅱ中最佳工艺为8倍量70%乙醇

提取温度为80℃

提取3次

每次1.0 h。结论: 此提取工艺合理可行

有效成分提取率高

为生产复方四黄栓提供参考。

Abstract

Objective:To optimize preparation technology of Fufang Sihuang suppository. Method:To improve extraction rate of active ingredients

technology was divided into alcohol extraction Ⅰand alcohol extraction Ⅱ

while single-factor test and orthogonal test was adopted to optimize preparation conditions which 70% ethanol used as extraction solvent

by using berberine as qualitycontrol criteria of alcohol extractionⅠand baicalin as qualitycontrol criteria of alcohol extraction Ⅱ to optimize extraction technology. Result:Optimum technology for alcohol extraction Ⅰwas as follows:extracted 3 times with 8

6 times the amount of 70% ethanol

extracted 1 h each time. Optimum technology for alcohol extraction Ⅱ was as follows:extracted three times with adding 8 times the amount of 70% ethanol for 1 h each time at 80 ℃. Conclusion:This extraction process was reasonable

practicable

high extraction rate of active ingredients

it could provide a reference for production of Fufang Sihuang suppository.

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Research Center for Differentiation and Development of Traditional Chinese Medicine （TCM） Basic Theory， Jiangxi Province Key Laboratory of TCM Etiopathogenisis， Jiangxi University of Chinese Medicine

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