Study on Quality Standard for Shenling Jianti Powder

ZHANG Wei; LI Wen-li; DING Ye; LI Xiao-yan; LUO Yan

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Study on Quality Standard for Shenling Jianti Powder

更新时间：2024-01-04

- Study on Quality Standard for Shenling Jianti Powder
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 2, Pages: 83-85(2012)
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- Published：2012
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ZHANG Wei, LI Wen-li, DING Ye, et al. Study on Quality Standard for Shenling Jianti Powder[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(2): 83-85.
DOI：

ZHANG Wei, LI Wen-li, DING Ye, et al. Study on Quality Standard for Shenling Jianti Powder[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(2): 83-85. DOI：

摘要

目的: 提高完善参苓健体散的质量标准。方法: 采用薄层色谱法对方中白术、甘草进行定性鉴别;采用高效液相色谱法测定甘草中甘草苷含量

色谱柱为Diamosil C18(4.6 mm×250 mm

5 μm)

流动相乙腈-0.5%冰醋酸(10∶90)

流速1.0 mL·min-1

检测波长276 nm。结果: 薄层色谱鉴别专属性强

重复性良好。甘草苷在0.037 08~0.370 8 μg有良好的线性关系(r=0.999 8)。平均回收率为101.6%

RSD 1.9%(n=6)。结论: 本方法简便、可靠、准确

可用于参苓健体散的质量控制。

Abstract

Objective: To improve the quality standard for Shenling Jianti Powder. Method: Rhizoma Atractylodis Macrocephalae and Radix Glycyrrhizae were indentified by TLC. The content of liquiritin in Radix Glycyrrhizae was determined by HPLC. The HPLC system consisted of Diamosil C18(4.6 mm×250 mm

5 μm)

acetonitrile-0.5%acetic acid(10∶90)as mobile phase

flow rate of 1.0 mL·min-1

detection wavelength at 276 nm. Result: The method of TLC was simple with strong specificity and good reproducibility. The linear range of liquirtin was 0.037 08-0.370 8 μg(r =0.9998). The average recovery rate was 101.6% and RSD was 1.9%(n=6). Conclusion: The developed method is simple

accurate and suitable for the quality control of Shenling Jianti Powder.

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Related Author

NIU Zheng-rui

MAO Shu-jie

GU Xue-zhu

LIU Hong-yu

LI Xian-duan

SHI Tao1

MENG Xian-sheng2

Related Institution

Hubei Institute for Food and Drug Control

Gansu Province Hospital of Traditional Chinese Medicine

Acupuncture and Moxibustion Hospital Affiliated to Anhui College of Traditional Chinese Medicine & Anhui Modern Engineering Technology Research Center of Chinese Medicine

Shanxi Renyuantang Pharmaceutical Co.,Ltd.

Shanxi University of Traditional Chinese Medicine

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