Study on Quality Standard of Yixin Badiranjibuya Granules

WANG Yun-fei; XING Jian-guo; HE Cheng-hui; XUE Gui-peng

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Study on Quality Standard of Yixin Badiranjibuya Granules

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- Study on Quality Standard of Yixin Badiranjibuya Granules
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 1, Pages: 87-89(2012)
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- Published：2012
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WANG Yun-fei, XING Jian-guo, HE Cheng-hui, et al. Study on Quality Standard of Yixin Badiranjibuya Granules[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(1): 87-89.
DOI：

WANG Yun-fei, XING Jian-guo, HE Cheng-hui, et al. Study on Quality Standard of Yixin Badiranjibuya Granules[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(1): 87-89. DOI：

摘要

目的 :建立益心巴迪然吉布亚颗粒的质量控制方法。方法 :采用薄层色谱法对颗粒中香青兰进行定性鉴别;采用HPLC方法测定香青兰中田蓟苷的含量。结果 :TLC定性鉴别重复性好

阴性无干扰;田蓟苷在0.101 8~1.221 μg线性关系良好(r=0.999 9)。平均加样回收率为99.29%

RSD为1.96%(n=9)。结论 :该方法专属性强

灵敏度高

重复性好

可用于该颗粒的质量控制。

Abstract

Objective : To establish the quality standard of Yixin Badiranjibuya Granules. Method : Thin-layer chromatography was used to identify Dracocephalum moldavica L. The content of tilianin from D. moldavica was determined by HPLC. Result : The specialization and reproducibility of the TLC methord was good. The linear range of tilianin was 0.101 8-1.221 μg(r=0.999 9).The average recovery rate was 99.29%(RSD 1.96%

n=9). Conclusion : The methord can control the quality of Yixin Badiranjibuya granules effectively.

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Related Institution

Hubei Institute for Food and Drug Control

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