GC-MS Analysis of Liposoluble Constituents from Herba Gueldenstaedtiae Vernae

LIU Hong-yan; ZHANG Yong-qing

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GC-MS Analysis of Liposoluble Constituents from Herba Gueldenstaedtiae Vernae

更新时间：2024-01-04

- GC-MS Analysis of Liposoluble Constituents from Herba Gueldenstaedtiae Vernae
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 2, Pages: 121-123(2012)
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- Published：2012
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LIU Hong-yan, ZHANG Yong-qing. GC-MS Analysis of Liposoluble Constituents from Herba Gueldenstaedtiae Vernae[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(2): 121-123.
DOI：

LIU Hong-yan, ZHANG Yong-qing. GC-MS Analysis of Liposoluble Constituents from Herba Gueldenstaedtiae Vernae[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(2): 121-123. DOI：

摘要

目的: 应用气相色谱-质谱法(GC-MS)分析甜地丁脂溶性化学成分。方法: 采用石油醚提取甜地丁中的脂溶性成分

气相色谱-质谱联用技术对所得的脂溶性成分进行分析。结果: 共鉴定出22个成分

占脂溶性成分总量的98.12%。其中含量较高成分为3-异辛氧基丙胺(23.178%)

α-脱氢孤挺花宁碱(20.388%)

2-甲氧基苯硫酚(11.387%)

3-甲基十七烷(9.278%)

(Z)-3-十六烯(7.000%)。结论: 甜地丁脂溶性成分中含烷、烯、酮、酚、醇、醛、酯类等多种化学成分

具有较高的医药、食品应用价值

分析结果为甜地丁资源的进一步开发利用提供了科学依据。

Abstract

Objective: The liposoluble constituents from Herba Gueldenstaedtiae Vernae were analyzed by GC-MS. Method: The liposoluble constituents were extracted by solvents petroleum ether and further identified by GC-MS and their relative content was calculated by area normalization method. Result: Through comparison with mass spectra database

twenty-two components

which accounted for 98.12% of the peak areas

were separated and identified. The major components were 3-(2-ethylhexyloxy)-propylamine (23.178%)

α-dihydrocaranine (20.388%)

2-methoxy benzenethiol (11.387%)

3-methylheptadecane (9.278%)

(Z)-3-hexadecene (7.000%). Conclusion: The liposoluble constituents have high application value in medicine and food industry and mainly consisted of alkane

olefin

ketone

phenol

alcohol

aldehyde

ester

etc. The present experiments provided a scientific basis for the further exploitation and utilization of this herb.

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Related Institution

Shandong University of Traditional Chinese Medicine,Ji’nan

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