Determination of Geniposide in Biyuanshu Granules by HPLC

WAN Jun

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Determination of Geniposide in Biyuanshu Granules by HPLC

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- Determination of Geniposide in Biyuanshu Granules by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 19, Pages: 78-80(2011)
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- Published：2011
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WAN Jun. Determination of Geniposide in Biyuanshu Granules by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(19): 78-80.
DOI：

WAN Jun. Determination of Geniposide in Biyuanshu Granules by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(19): 78-80. DOI：

摘要

目的: 建立高效液相色谱法测定鼻渊舒颗粒中栀子苷含量的方法。方法: 采用Kromasil C18(4.6 mm×150 mm

5 μm)色谱柱

流动相甲醇-0.2%磷酸溶液(30 ∶70)

流速1.0 mL·min-1

检测波长238 nm

柱温35 ℃。结果: 栀子苷在0.04~0.51 μg(r=0.999 9)

线性关系良好。平均回收率100.35%(n=5)

RSD 1.31%。结论: 方法分离度好

快速、简便

适用于鼻渊舒颗粒中栀子苷的含量测定

可作为产品的质量控制方法。

Abstract

Objective: To establish a HPLC method for determination of geniposide in Biyuanshu granules. Method: The Kromasil C18 column(4.6 mm×150 mm

5 μm)was used

and mobile phase was composed of CH3OH-0.2% H3PO4(30 ∶70). Detection wavelength was at 238 nm

the flow rate was 1.0 mL·min-1

column temperature was at 35 ℃. Result: The linear response range was from 0.04-0.51 μg(r=0.999 9).The recovery rate was 100.35%(n=5)

RSD was 1.31%. Conclusion: The HPLC method is simple

accurate

and suitable for the determination of geniposide in Biyuanshu granules.

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Related Author

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ZHANG Pei-qin

SU Song-bai

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LI Xiang

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Related Institution

The First Affiliated Hospital of Guiyang College of Traditional Chinese Medicine

Shuguang Hospital， Institute of Liver Diseases， Key Laboratory of Liver and Kidney Disease （Ministry of Education）， Shanghai Key Laboratory of Traditional Chinese Clinical Medicine，Shanghai University of Traditional Chinese Medicine （TCM）

Institute of Chinese Materia Medica， Institute of Interdisciplinary Integrative Medicine， Shanghai University of TCM

Key Laboratory of Modern Preparation of TCM Ministry of Education， Jiangxi University of TCM

School of Pharmacy，Jiangxi University of Traditional Chinese Medicine

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