Extraction Process of Solamargine from

ZHANG Yan; XU Lian-ming; CHEN Xiang; CHEN Jun; MENG Zao-qing; XIAO Wei

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Extraction Process of Solamargine from

更新时间：2024-01-04

- Extraction Process of Solamargine from
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 17, Pages: 5-7(2011)
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- Published：2011
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ZHANG Yan, XU Lian-ming, CHEN Xiang, et al. Extraction Process of Solamargine from [J]. Chinese journal of experimental traditional medical formulae, 2011, 17(17): 5-7.
DOI：

ZHANG Yan, XU Lian-ming, CHEN Xiang, et al. Extraction Process of Solamargine from [J]. Chinese journal of experimental traditional medical formulae, 2011, 17(17): 5-7. DOI：

摘要

目的: 研究龙葵药材中澳洲茄边碱的最佳提取工艺。方法: 以澳洲茄边碱提取率为指标

采用L9 (34)正交试验

考察乙醇体积分数、料液比、提取时间及提取次数对提取率的影响

优选出最佳的提取工艺。用高效液相法测定澳洲茄边碱的含量。结果: 优选出的澳洲茄边碱最佳提取工艺为用80%乙醇20倍量回流提取2次、每次4 h。结论: 提取工艺合理可行

适用于龙葵中澳洲茄边碱的提取。

Abstract

Objective: To study the optimum extracting process of solamargine from Solanum nigrum Method: The optimum extraction process was investigated by L9(34) orthogonal design with the yield of solamargine as index

and four factors were chosen

including ethanol concentration

solid-liquid ratio

extraction times and extraction time. HPLC was used to determine the content of solamargine. Result: The optimum extraction conditions was to reflux the herbs for two times

four hours each time with 20 times amount of 80% ethanol. Conclusion: The selected technology is reasonable and feasible

and was suitable for extraction of solamargine.

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