Study on the Quality Standard for Yimei Lotion

WU Xiao-yan; TANG Ai-cun; XIE Zhen; CHEN Yong; ZENG Hai-sheng

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Study on the Quality Standard for Yimei Lotion

更新时间：2024-01-04

- Study on the Quality Standard for Yimei Lotion
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 18, Pages: 78-80(2011)
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- Published：2011
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WU Xiao-yan, TANG Ai-cun, XIE Zhen, et al. Study on the Quality Standard for Yimei Lotion[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(18): 78-80.
DOI：

WU Xiao-yan, TANG Ai-cun, XIE Zhen, et al. Study on the Quality Standard for Yimei Lotion[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(18): 78-80. DOI：

摘要

目的: 建立抑霉洗剂的质量控制方法。方法: 以苦参碱、氧化苦参碱为对照

采用TLC法鉴别该制剂中的苦参

并采用HPLC法测定制剂中苦参碱的含量。结果: 在TLC鉴别中能检出苦参

供试品与对照品、对照药材色谱在相应的位置上显相同的橙红色斑点

阴性对照无干扰。苦参碱在0.258 4~2.584 0 μg 线性关系良好

回归方程为Y=71.217 8 X -1 045.177 9(r=0.999 4)

平均回收率为97.89%。结论: 建立的制剂质量控制方法简便、可靠、准确

可作为该制剂的质量控制方法。

Abstract

Objective: To establish the quality standard for Yimei lotion. Method: Sophorae Flavescentis Radix was identified by TLC with ammothamnine and matrine as the standard. The content of matrine in Yimei lotion was determined by HPLC. Result: Sophorae Flavescentis Radix could be identified by TLC; The linearity of matrine was good in the range of 0.258 4-2.584 0 μg

regress equation was Y =71.217 8 X -1 045.177 9

r=0.999 4; the average recovery was 97.89%. Conclusion: The method of TLC identification and HPLC determination is simple

reliable and accurate which can be used for the quality control of Yimei lotion.

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