Determination of Dehydrodiisoeugenol in Nutmeg Roasted with Wheat Bran by RP-HPLC

YUAN Zi-min; CHEN Jian-feng; JIA Tian-zhu

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Determination of Dehydrodiisoeugenol in Nutmeg Roasted with Wheat Bran by RP-HPLC

更新时间：2024-01-04

- Determination of Dehydrodiisoeugenol in Nutmeg Roasted with Wheat Bran by RP-HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 18, Pages: 60-61(2011)
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- Published：2011
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YUAN Zi-min, CHEN Jian-feng, JIA Tian-zhu. Determination of Dehydrodiisoeugenol in Nutmeg Roasted with Wheat Bran by RP-HPLC[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(18): 60-61.
DOI：

YUAN Zi-min, CHEN Jian-feng, JIA Tian-zhu. Determination of Dehydrodiisoeugenol in Nutmeg Roasted with Wheat Bran by RP-HPLC[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(18): 60-61. DOI：

摘要

目的: 建立麸煨肉豆蔻饮片中去氢二异丁香酚的含量测定方法。方法: 采用高效液相色谱法

以甲醇-水 (75∶25)为流动相

柱温为室温

检测波长为274 nm。结果: 去氢二异丁香酚的进样量在0.075~0.60 μg呈现良好现性关系(r=0.999 9)

平均回收率为98.22%(n=6)

RSD为1.9%。结论: 采用高效液相色谱法测定麸煨肉豆蔻饮片中去氢二异丁香酚的含量

方法简便、灵敏、准确

可用于麸煨肉豆蔻饮片的质量控制。

Abstract

Objective: To establish HPLC for determining the content of dehydrodiisoeugenol in Nutmeg roasted with wheat bran. Method: An HPLC method was developed. The chromatographic conditions were as follows: Diamonsil C18 column and methanol-water (75∶25) as mobile phase

detection wavelength at 274 nm. Result: The linear range of dehydrodiisoeugenol was 0.075-0.60 μg(r=0.999 9). The average recovery rate was 98.22% and RSD was 1.9%. Conclusion: The method is simple and accurate with good repeatability

and can be used for determination of dehydrodiisoeugenol in Nutmeg roasted with wheat bran.

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Related Institution

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