Study on Optimum Technology of Ethanol Percolation Extraction for Citri Grandis Exocarpium Plaster by Orthogonal Test
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Study on Optimum Technology of Ethanol Percolation Extraction for Citri Grandis Exocarpium Plaster by Orthogonal Test
Chinese Journal of Experimental Traditional Medical FormulaeVol. 17, Issue 6, Pages: 38-40(2011)
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Published:2011
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WANG Lan-fang, FANG You-ni, HAN Jian-wei, et al. Study on Optimum Technology of Ethanol Percolation Extraction for Citri Grandis Exocarpium Plaster by Orthogonal Test[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(6): 38-40.
DOI:
WANG Lan-fang, FANG You-ni, HAN Jian-wei, et al. Study on Optimum Technology of Ethanol Percolation Extraction for Citri Grandis Exocarpium Plaster by Orthogonal Test[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(6): 38-40.DOI:
Study on Optimum Technology of Ethanol Percolation Extraction for Citri Grandis Exocarpium Plaster by Orthogonal Test
渗漉速度5 mL ·min-1 ·kg-1。3批验证试验化橘红中柚皮苷平均转移率为79.0%。 结论: 优选的提取工艺合理
转移率较高。
Abstract
Objective: To optimize the technical conditions of ethanol percolation extraction for Citri Grandis Exocarpium Plaster. Method: The content of naringin extracted from Citri Grandis Exocarpium
which was regarded as the marker of detection
was determined by high performance liquid chromatography and was used to optimize the extraction processing conditions by L9(34) orthogonal test. Result: The optimum extraction condition was that the concentration of ethanol was 80%
the volume of solvent was 15 times of medicinal materials
the soaking time was 24 hours and the percolating speed was 5 mL ·min-1 ·kg-1. The average transferring rate of naringin in 3 batches of samples was 79.0%. Conclusion: The optimum extraction process is reasonable and the transferring rate of naringin is higher.
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Related Institution
Liaoning University of Traditional Chinese Medicine,Liaoning Province Traditional Chinese Medicine Engineering Research Center
Sixth People’s Hospital of Dalian Pharmacy
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