Identification of  by HPLC Fingerprint

YANG Li-yong; LI Yu-sheng; WANG Xiang-pei; YANG Ye; WU Hong-mei; JIN Feng-yun

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Identification of by HPLC Fingerprint

更新时间：2024-01-04

- Identification of by HPLC Fingerprint
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 8, Pages: 104-107(2011)
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- Published：2011
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YANG Li-yong, LI Yu-sheng, WANG Xiang-pei, et al. Identification of by HPLC Fingerprint[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(8): 104-107.
DOI：

YANG Li-yong, LI Yu-sheng, WANG Xiang-pei, et al. Identification of by HPLC Fingerprint[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(8): 104-107. DOI：

摘要

目的: 建立菝葜药材高效液相色谱(HPLC)指纹图谱鉴别方。方法: 采用RP-HPLC

以Diamonsil-C18(4.6 mm×250 mm

5 μｍ)色谱柱为分析柱

流动相乙腈-0.1%磷酸水

梯度洗脱

流速0.6 mL ·min-1

330 nm波长下测定菝葜、光叶菝葜的指纹图谱

并作相似度比较分析。结果: 建立了菝葜药材HPLC指纹图谱共有模式

18个共有指纹峰被标定

并对菝葜与光叶菝葜药材的HPLC指纹图谱进行相似度比较

结果具有明显差异。结论: HPLC指纹图谱具有方法简便

重复性好

特征性强的特点

可用于菝葜药材的鉴别。

Abstract

Objective: To establish a HPLC fingerprint for the identification of Smilax china. Method: The analysis was carried out on a Diamonsil C18(4.6 mm×250 mm

5 μｍ)with a mobile phase consisting of acetonitrile-0.1 % phosphoric acid

gradient eluent

the flow rate of 0.6 mL ·min-1. The wave length was 330 nm

data were analyzed by fingerprint similarity evalution software to compare the similarity of samples. Result: The mutual mode to HPLC fingerprints was estabilished

and the 18 mutual peaks were indicated.The similarities among the of S. china and S. glabra collected from different sources were obtained. there were apparent difference in fingerprint. Conclusion: HPLC fingerprint method is repeatable and feasible and can be suitable for identifying Musa basjoo.

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Related Institution

Guiyang College of Traditional Chinese Medicine

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Guangdong Provincial Enterprise Key Laboratory of Traditional Chinese Medicine Formula Granule，Guangdong Efong Pharmaceutical Co. Ltd.

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