Quality standard for Mangankang Pills

SHI Jun-han; NIU Xiao-jing; SUN Ming-ming

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Quality standard for Mangankang Pills

更新时间：2024-01-04

- Quality standard for Mangankang Pills
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 16, Pages: 42-44(2010)
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- Published：2010
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SHI Jun-han, NIU Xiao-jing, SUN Ming-ming. Quality standard for Mangankang Pills[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(16): 42-44.
DOI：

SHI Jun-han, NIU Xiao-jing, SUN Ming-ming. Quality standard for Mangankang Pills[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(16): 42-44. DOI：

摘要

目的 :建立慢肝康丸质量标准。方法 :采用薄层色谱法(TCL)对慢肝康丸中的当归、白术、黄芪、柴胡进行定性鉴别;用HPLC测定慢肝康丸中芍药苷的含量。结果 :薄层色谱鉴别法专属性强

阴性无干扰;芍药苷在0.005 8~0.116 μg线性关系良好

得到回归方程Y=1.07×106X-7.79×103(r=0.999 9)。平均加样回收率为98.6% (n=6

RSD 1.19%)。结论 :方法简便

灵敏度高

结果准确

可有效控制慢肝康丸的质量。

Abstract

Objective: To establish quality standard of Mangankang pills. Method: Angelica sinensis

Atractylodis Macrocephalae Rhizoma

Astragali and Bupleurum were identified by TLC.The content of paeoniflorin of Paeonine Radix Alba in the Mangankang pills was determined by HPLC. Result: TLC method was specific for the identification of Angelica sinensis

Atractylodes

Astragalus and Bupleurum

and no interference was found for negatives.Paeoniflorin was linear in the range of 0.058~1.16 μg.The regression equation was Y=1.07×106X-7.78×103(r=0.999 9).The average recovery was 98.6% (n=6

RSD 1.19%). Conclusion: This method is convenient

accurate

higher sensitivity

and can be used for controling the quality of Mangankang pills.

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Related Author

JIANG Zhen-ou1

LIU Zhi-sheng1

HUANG Rui-song2

WEI Shan-xin1

HUANG Min-gui1

QIN Lan-fang1

CHEN Ping1

LI Zhuo-ming2

Related Institution

Taiyuan Institute for Food and Drug Control,Taiyan

Shanxi Pharmaceutical Occupational College,Taiyan

Shanxi Shuangren Pharmaceutical Co.Ltd

School of Life Science and Engineering,Southwest Jiaotong University

The First Affiliated Hospital Guangzhou University of Traditional Chinese Medicine

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