Chromatographic Corresponding Identifications in Different Botanical Origins of Sinapis Semen

ZHANG Cun; LI Li; XIAO Yong-qing; PANG Zhen; LI Gui-liu; MA Yin-lian

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Chromatographic Corresponding Identifications in Different Botanical Origins of Sinapis Semen

更新时间：2024-09-23

- Chromatographic Corresponding Identifications in Different Botanical Origins of Sinapis Semen
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 14, Pages: 38-40(2010)
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- Published：2010
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ZHANG Cun, LI Li, XIAO Yong-qing, et al. Chromatographic Corresponding Identifications in Different Botanical Origins of Sinapis Semen[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 38-40.
DOI：

ZHANG Cun, LI Li, XIAO Yong-qing, et al. Chromatographic Corresponding Identifications in Different Botanical Origins of Sinapis Semen[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 38-40. DOI：

摘要

目的: 研究建立芥子不同品种的化学色谱对应鉴别方法。方法: 以4-羟基-苄基芥子苷、4-羟基苯甲酰胆碱和芥子碱复盐为对照品

采用TLC和HPLC鉴别。结果: 黄芥子、白芥子的TLC和HPLC图谱有明显差异

白芥子能检出3个对照品

黄芥子仅能检出芥子碱复盐

2种色谱方法鉴定结果一致。结论: 所建立的TLC和HPLC图谱鉴别方法简便易行

可以快速地鉴别区分黄芥子和白芥子

为芥子不同品种的质量评价方法提供了试验依据。

Abstract

Objective : To study on the chemical chromatographic corresponding methods in different botanical origins of Sinapis semen. Method : The presence of 4-hydroxybenzylglucosinolate

4-hydroxy benzoylcholine and sinapine was identified by TLC and HPLC

respectively. Result : The TLC and HPLC chromatograms showed the obvious differences between the two origins

while three standards were identified in Sinapis alba

and only sinapine was detected in Brassica juncea . Conclusion : The established methods were simple and can be used for evaluating the quality in different botanical origins of Sinapis semen.

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Related Author

ZHANG Cun

LI Li

XIAO Yong-qing

PANG Zhen

LI Gui-liu

MA Yin-lian

LI Man-ling

FENG Wei-hong

Related Institution

Institute of Chinese Materia Madica,China Academy of Chinese Medicial Sciences

Hubei Institute for Food and Drug Control

Natural Pharmaceutical R&D

修正药业长春高新制药有限公司

吉林省中医药科学院

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