Studies on the Quality standard of Bimintong Capsule

CHENG Yao-tang; MA Yan

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Studies on the Quality standard of Bimintong Capsule

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- Studies on the Quality standard of Bimintong Capsule
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 5, Pages: 70-72(2010)
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- Published：2010
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CHENG Yao-tang, MA Yan. Studies on the Quality standard of Bimintong Capsule[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(5): 70-72.
DOI：

CHENG Yao-tang, MA Yan. Studies on the Quality standard of Bimintong Capsule[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(5): 70-72. DOI：

摘要

目的: 建立鼻敏通胶囊的质量标准。方法: 采用TLC法鉴别方中的川芎、独活和防风。用HPLC法测定蛇床子素的含量

采用Shim-Pack ODS 柱(4.6 mm×150 mm

5 μm);流动相为乙腈-水(60 ∶40)

检测波长322 nm

流速1.0 mL ·min-1。结果: TLC色谱法检出川芎、独活和防风

阴性对照无干扰。蛇床子素浓度在5.68~56.80 μg ·mL-1范围内线性关系良好(r=0.999 8)。平均回收率为99.27%

RSD=1.01%(n=6)。结论: 建立的TLC和HPLC方法专属性强、灵敏度高、重复性好

可用于鼻敏通胶囊的质量控制。

Abstract

Objective: To establish the quality standard of Bimintong Capsule. Method: Rhizoma chuanxiong

Radix Angelicae pubescentis

and Radix saposhnikoviae were identified by TLC. The HPLC method was established to determine the content of osthole. A Shim-Pack ODS column was used with acetonitrile-water(60 ∶40) as mobile phases. The flow rate was 1.0 mL ·min-1. The detection wavelength was at 322 nm. Result: Rhizoma chuanxiong

Radix Angelicae pubescentis

and Radix saposhnikoviae could be identified by TLC and there were noninterference of the negative controls. Osthole was linear in the range of 5.68~56.80 μg ·mL-1(r=0.999 8).The average recovery was 99.27%

and RSD 1.01%(n=6). Conclusion: The method established can be used as quality control for Bushen Jianpi Granule.

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Related Author

CHENG Yao-tang

MA Yan

SHI Tao1

MENG Xian-sheng2

LUO Guo-an2

WANG Yi-ming2

Related Institution

Acupuncture and Moxibustion Hospital Affiliated to Anhui College of Traditional Chinese Medicine & Anhui Modern Engineering Technology Research Center of Chinese Medicine

Hubei Institute for Food and Drug Control

Gansu Province Hospital of Traditional Chinese Medicine

Shanxi Renyuantang Pharmaceutical Co.,Ltd.

Shanxi University of Traditional Chinese Medicine

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