Determination of Adenosine in Weigan Effervescent Tablets by RP-HPLC

MAO Yan; YANG Wei-jun; MA Yila·maimaitiyiming; HE Jin-hua

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Determination of Adenosine in Weigan Effervescent Tablets by RP-HPLC

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- Determination of Adenosine in Weigan Effervescent Tablets by RP-HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 2, Pages: 26-27(2010)
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- Published：2010
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MAO Yan, YANG Wei-jun, MA Yila·maimaitiyiming, et al. Determination of Adenosine in Weigan Effervescent Tablets by RP-HPLC[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(2): 26-27.
DOI：

MAO Yan, YANG Wei-jun, MA Yila·maimaitiyiming, et al. Determination of Adenosine in Weigan Effervescent Tablets by RP-HPLC[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(2): 26-27. DOI：

摘要

目的:采用RP-HPLC法建立维感泡腾片中腺苷的含量测定方法。方法:以甲醇-水(8∶92)为流动相

ShimadzuC18(250 mm×4.6 mm

S-5 μm)色谱柱

检测波长为260 nm

柱温为35 ℃

流速为1.0 mL·min-1。结果:腺苷在4.3~33.8 μg范围内呈良好的线性关系(r=0.999 7)

腺苷的平均回收率为101.0%(n=9

RSD=1.4%)。结论:该方法快速简便易行

重复性良好

结果准确

可作为维感泡腾片中腺苷质量评价的方法。

Abstract

Objective:To develop a RP-HPLC method for the quantification of adenosine in Weigan Effervescent Tablets. Methods: The analysis was carried out on a Shimadzu C18 column(250 mm×4.6 mm

S-5 μm)and the mobile phase was a mitture of methanol-water(8∶92)with a flow rate of 1.0 mL· min-1.The detection wavelength was 260 nm

and the column temperature was 35 ℃. Results: The linear response ranges of adenosine was 4.3~33.8 μg(r=0.999 7)

and the average recovery was 101.0%(n=9

RSD=1.4%). Conclusion: The method is quick

simple and reproducible for the determination of adenosine in Weigan Effervescent Tablets.

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Related Author

MAO Yan

YANG Wei-jun

MA Yila·maimaitiyiming

HE Jin-hua

WANG Guo-hua

LI Hui

NIE Qi-xia

ZANG chen

Related Institution

Xinjiang Institute of Materia Medica,Urmiqu

Medical College of Shaoguan University

Shaoguan Institute for Drug Control

School of Pharmacy,Anhui Medical University

Department of Pharmacy,Third-Grade pharmaceutical Chemistry Laboratory of State Administration of Traditional Chinese Medicine,The First Affiliated Hospital of Anhui Medical University

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