Determination of astragnaloside Ⅳ in zhuaikang capsule by HPLC-ELSD

SUN Jian; LIU Hong; FAN Bin

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Determination of astragnaloside Ⅳ in zhuaikang capsule by HPLC-ELSD

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- Determination of astragnaloside Ⅳ in zhuaikang capsule by HPLC-ELSD
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 4, Pages: 60-62(2010)
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- Published：2010
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SUN Jian, LIU Hong, FAN Bin. Determination of astragnaloside Ⅳ in zhuaikang capsule by HPLC-ELSD[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(4): 60-62.
DOI：

SUN Jian, LIU Hong, FAN Bin. Determination of astragnaloside Ⅳ in zhuaikang capsule by HPLC-ELSD[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(4): 60-62. DOI：

摘要

目的 : 建立中药复方祝艾康胶囊中黄芪甲苷的含量测定方法。方法 : 采用Diamonsil C18色谱柱(4.6 mm×250 mm

5 μm)

乙腈-水(33 ∶67)为流动相

流速1.0 mL ·min-1

柱温35 ℃

漂移管温度105 ℃

空气流速2.7 L ·min-1。结果 : 黄芪甲苷在1.515~7.575 μg具良好的线性关系(r=0.999 96)

平均回收率98.83

RSD 1.8%。结论 : 该法准确、可靠、重复性好

可用于控制祝艾康胶囊的质量。

Abstract

Objective: To establish a method of determining the content of astragaloside IV in Zhuaikang Capsule. Method: The separation was performed on a Diamonsil C18(250 mm×4.6 mm

5 μm)column with acetonitrile-water(33 ∶67) as the mobile phase. The flow rate was 1.0 mL ·min-1. Temperature of drift tube was set at 105 ℃. The gas flow rate was at 2.7 L ·min-1. Result: Astragaloside IV was linear in the range of 1.515~7.575 μg(r=0.999 96). The average recovery rate of astragaloside IV was 98.83%

RSD 1.8%. Conclusion: This method is sensitive

accurate

and simple with little interference for the determination of astragaloside IV content. The method can be used for controlling the quality of Zhuaikang Capsule.

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Related Author

LIU Hong2

FAN Bin1

SUN Jian1

WANG Zhuxin2

WU Yong1

LIU Wen-long1

HE Fu-yuan1

Related Institution

Experimental Research Center,China Academy of Chinese Medical Sciences

Institute of Basic Theory of Traditional Chinese Medicine,China Academy of Chinese Medical Sciences

Anhui Academy of Medical Sciences

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