Analysis of Volatile Chemical Constituents in Entire Plants of  by GC-MS Spectrometry

HE Qian-song; FENG Yong; PENG Quan-cai; YANG Zhan-nan

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Analysis of Volatile Chemical Constituents in Entire Plants of by GC-MS Spectrometry

更新时间：2024-01-04

- Analysis of Volatile Chemical Constituents in Entire Plants of by GC-MS Spectrometry
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 9, Pages: 83-87(2010)
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- Published：2010
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HE Qian-song, FENG Yong, PENG Quan-cai, et al. Analysis of Volatile Chemical Constituents in Entire Plants of by GC-MS Spectrometry[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(9): 83-87.
DOI：

HE Qian-song, FENG Yong, PENG Quan-cai, et al. Analysis of Volatile Chemical Constituents in Entire Plants of by GC-MS Spectrometry[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(9): 83-87. DOI：

摘要

目的 :运用GC-MS分析臭常山根、茎及叶的主要挥发性化学成分

并比较其成分种类的异同与含量差异。方法 :采用固相微萃取(head-space solid-phase microextraction

SPME)技术分别提取臭常山根、茎及叶的主要挥发性化学成分

用GC-MS对其挥发性成分进行鉴定。结果 :从臭常山根、茎及叶中分离出85个峰

共鉴定了83个化合物。根的主要挥发性成分有1-甲基-5

6-二乙烯基-1-环己烯(80.70%)和3-甲基-3

4-二乙烯基-1-环己烯(7.59%)

茎的主要挥发性成分有α-蒎烯(36.12%)、苄基异腈(14.46%)、苯乙基异氰(12.57%)、甲基辛基酮(4.59%)

叶的主要挥发性成分有2-己烯醛(21.11%)、Diktaminin(19.00%)、桧烯(10.79%)及氧化石竹烯(6.25%)。结论 :臭常山根、茎及叶所含挥发性成分差异较大

共有成分11个(分别占根、茎、叶挥发性成分的93.15%

51.82%和20.33%)

为进一步研究和运用臭常山根、茎及叶入药提供了参考。

Abstract

Objective: To analyze and compare the volatile components which were extracted from entire plants of Orixa japonica . Method: The volatile components were extracted from entire plants of Orixa japonica Thunb. by the methods of SPME and the chemical components of them were identified by GC-MS. Result: Eighty-five compounds were extracted from entire plants of Orixa japonica

eighty-three compounds were identified. The main volatile components of root are 1-methyl-5

6-divinyl-1-cyclohexene(80.70%) and 3-methyl-3

4-divinyl-1-cyclohexene (7.59%)

the main volatile components of stem are α-pinene(36.12%)

benzyl is onitrile(14.46%)

Benzyl is ocyanide (12.57%) and 2-decanone (4.59%)

the main volatile components of leaf are 2-Hexenal (21.11%)

diktaminin(19.00%)

sabinen(10.79%) and caryophyllene oxide (6.25%). Conclusion: Contain volatile components in the entire plants of Orixa japonica are quite different

eleven compounds were common in both of root

stem and leaf. The results of the studies can be referenced when the entire plants of Orixa japonica need to be further studied.

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Related Institution

Institute of Chinese Material Medica，China Academy of Chinese Medical Sciences

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南阳理工学院,南阳理工学院,河南省南阳市宛城区南阳理工学院张仲景国医学院,南阳理工学院

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