Determination of Rutin in Motherwort Herb and Herbs with Same Action by HPLC

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Determination of Rutin in Motherwort Herb and Herbs with Same Action by HPLC

更新时间：2024-01-04

- Determination of Rutin in Motherwort Herb and Herbs with Same Action by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 15, Issue 10, Pages: 6-7(2009)
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- Published：2009
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Determination of Rutin in Motherwort Herb and Herbs with Same Action by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(10): 6-7.
DOI：

Determination of Rutin in Motherwort Herb and Herbs with Same Action by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(10): 6-7. DOI：

摘要

目的:建立益母草及其习用药材中芦丁的HPLC含量测定方法。方法:采用Kromasil C18柱(4.6mm×150mm

5μm)

流动相为甲醇-0.5%磷酸(33∶67)

流速为1.0mL·min-1

检测波长为254nm

柱温30℃。结果:芦丁线性范围为(0.075～0.375)μg

r=0.9996

平均回收率为96.62%

RSD为0.99%。结论:该方法快速、简便、准确、重复性较好

结果可靠

可用于控制益母草及其习用药材的质量。

Abstract

Objective:To develop an HPLC method for the determination of rutin in Motherwort Herb and herbs with the same action.Methods: Analyses were carried out on an Kromasil C18(4.6 mm×150 mm

5 μm)column at 30℃ eluted with a mobile phase consisting of methanol-0.5%phosphoric acid(33∶67)and detected at 254 nm.The flow rate was 1.0 mL·min-1.Results: The linear range of rutin was 0.075～0.375 μg·mL-1.The average recovery was 96.62%(RSD=0.99%).Conclusion: The method is simple and accurate

and can be used for the quality control of Motherwort herb and the herbs with the same action.

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Related Author

WANG Guo-hua

LI Hui

NIE Qi-xia

ZANG chen

ZHANG Bao-xian

HAN Jian-wei1

LIU Ying2

WEI Yuan-feng1

Related Institution

Department of Pharmacy,Guiyang College of Traditional Chinese Medicine

School of Pharmacy,Anhui Medical University

Department of Pharmacy,Third-Grade pharmaceutical Chemistry Laboratory of State Administration of Traditional Chinese Medicine,The First Affiliated Hospital of Anhui Medical University

Xinjiang Institute of Materia Medica,Urmiqu

Guangzhou XinQqun Pharmaceutical CO.LTD Guangzhou

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