Salviae Miltiorrhizae Radix et Rhizoma by Infrared Spectroscopy

WANG Ling; GONG Mu-xin; WANG Zhi-min; WAN Kai-yang

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Salviae Miltiorrhizae Radix et Rhizoma by Infrared Spectroscopy

更新时间：2024-09-23

- Salviae Miltiorrhizae Radix et Rhizoma by Infrared Spectroscopy
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 5, Pages: 34-37(2010)
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- Published：2010
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WANG Ling, GONG Mu-xin, WANG Zhi-min, et al. Salviae Miltiorrhizae Radix et Rhizoma by Infrared Spectroscopy[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(5): 34-37.
DOI：

WANG Ling, GONG Mu-xin, WANG Zhi-min, et al. Salviae Miltiorrhizae Radix et Rhizoma by Infrared Spectroscopy[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(5): 34-37. DOI：

摘要

目的: 建立红外光谱技术

快速鉴别丹参药材产地及确定丹酚酸B含量高低。方法: 采集来自4个产地的40批丹参药材的红外光谱信息

寻找可以反映产地特征的二阶导数红外光谱特征峰

以及可进行丹酚酸B快速定量的原谱特征峰。结果: 不同产地丹参药材的二阶导数红外光谱特征吸收峰存在差异

可以反映丹参药材的不同产地;原谱1 262 cm-1峰的吸收峰高基本不受其他成分的影响

可以反映丹酚酸B含量且与液相色谱含量结果呈正相关

实现丹酚酸B的快速半定量。结论: 建立的红外光谱技术可以为中成药生产过程中

投料丹参药材的快速评价提供一种新的备选方法。

Abstract

Objective: To establish a fast method to evaluate the geographic origins of salviae miltiorrhizae radix et rhizoma and the contents of salvianolic acid B based on infrared spectroscopy (IR). Method: IR spectra of forty samples collected from 4 different origins were analyzed to search for the characteristic peaks on second derivative (2D) spectra to reflect the characteristics of origin

also to search for a characteristic peak on normalized spectra for fast quantitation of salvianolic acid B. Result: Some characteristic peaks on 2D spectra were found which reflect 4 different origins. The intensity of 1 262 cm-1 on normalized spectra was found to correlate well with the content of salvianolic acid B determined by high performance liquid chromatography

which realize the fast quantitative analysis of salvianolic acid B. Conclusion: The proposed IR method provides a new alternative of fast quality evaluation of salviae miltiorrhizae radix et rhizoma for manufacture of traditional Chinese medicine.

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Related Author

WANG Ling1

GONG Mu-xin1

WANG Zhi-min3

WAN Kai-yang3

TU Shuxin

WANG Yan

HE Xiaoli

SUN Ting

Related Institution

Institute of Chinese Materia Medica,China Academy of Chinese Medical Sciences

National Center of Traditional Chinese Medicines

Chinese Medical Institute,Capital Medical University

Institute of Medicinal Plant Development，Chinese Academy of Medical Sciences and Peking Union Medical College

Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

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