Qualitative and Quantitative Analysis of Xiegan Anshen Pills

XIAO Li-he1; GUO Qiao-ji1; GUAN Xiao-ying2; XIONG Ying1

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Qualitative and Quantitative Analysis of Xiegan Anshen Pills

更新时间：2024-01-04

- Qualitative and Quantitative Analysis of Xiegan Anshen Pills
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 15, Issue 8, Pages: 16-19(2009)
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- Published：2009
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XIAO Li-he1, GUO Qiao-ji1, GUAN Xiao-ying2, et al. Qualitative and Quantitative Analysis of Xiegan Anshen Pills[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(8): 16-19.
DOI：

XIAO Li-he1, GUO Qiao-ji1, GUAN Xiao-ying2, et al. Qualitative and Quantitative Analysis of Xiegan Anshen Pills[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(8): 16-19. DOI：

摘要

目的:建立泻肝安神丸的定性及定量方法。方法:采用薄层色谱法对制剂中的当归、栀子、黄芩、远志进行定性鉴别;采用高效液相色谱法测定制剂中龙胆苦苷的含量。结果:薄层色谱显色清晰且阴性对照无干扰。龙胆苦苷在0.0102～0.2040mg·mL-1浓度范围内呈良好的线性关系

平均回收率为98.2%

RSD=1.2%。结论:该法操作简便

结果准确

重复性好

可用于该制剂的质量控制。

Abstract

Objective:To develop the qualitative and quantitative methods for quality control of Xiegan Anshen pills.Methods: Radix Angelicae Sinensis

Fructus Gardeniae

Radix Scutellariae and Radix Polygalae were identified by TLC.HPLC was used for determination of gentiopicrin.Result: The TLC methods for Xiegan Anshen pills identification were specific with good separation.The linear range for quantitication of gentiopicrin was from(0.010 2) to (0.204 0 mg·mL-1)(r=(0.999 9)) and the mean recovery of gentioporin was 98.2%(RSD=1.2%).Conclusion: These methods were found to be reliable

accurate and specific

they can be used for the quality control of Xiegan Anshen pills.

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Related Author

JIANG Zhen-ou1

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HUANG Rui-song2

WEI Shan-xin1

HUANG Min-gui1

QIN Lan-fang1

ZHU Yu

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Related Institution

Taiyuan Institute for Food and Drug Control,Taiyan

Shanxi Pharmaceutical Occupational College,Taiyan

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School of Life Science and Engineering,Southwest Jiaotong University

The First Affiliated Hospital Guangzhou University of Traditional Chinese Medicine

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