Study on Qualitative and Quantitative Methods for Xuesaitong Dropping Pills

YAN Hui; ZHONG Lei; WANG Su-hui; WANG Rui; ZHAO Han-chen

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Study on Qualitative and Quantitative Methods for Xuesaitong Dropping Pills

更新时间：2024-01-04

- Study on Qualitative and Quantitative Methods for Xuesaitong Dropping Pills
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 14, Issue 11, Pages: 1-3(2008)
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- Published：2008
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YAN Hui, ZHONG Lei, WANG Su-hui, et al. Study on Qualitative and Quantitative Methods for Xuesaitong Dropping Pills[J]. Chinese journal of experimental traditional medical formulae, 2008, 14(11): 1-3.
DOI：

YAN Hui, ZHONG Lei, WANG Su-hui, et al. Study on Qualitative and Quantitative Methods for Xuesaitong Dropping Pills[J]. Chinese journal of experimental traditional medical formulae, 2008, 14(11): 1-3. DOI：

摘要

目的:制定血塞通滴丸的质量标准。方法:以薄层色谱(TLC)法进行定性鉴别

以高效液相色谱(HPLC)法测定人参皂苷Rg1、人参皂苷Rb1和三七皂苷R1

采用C18柱

流动相为乙腈-水系统梯度洗脱

检测波长:203nm

流速:1.0mL·min-1

柱温:室温。结果:TLC法可以很好地鉴别滴丸中的主要成分;HPLC法测定人参皂苷Rb1、人参皂苷Rg1的线性范围为0.2～1.0μg

三七皂苷R1的线性范围为0.1～0.5μg。其总平均回收率为97.93%。结论:方法可行

重复性好

可用于血塞通滴丸的质量控制。

Abstract

Objective:To develop the Qualitative and Quantitative Methods of Xuesaitong dropping pills.Methods:TLC method was used for identification.Ginsenoside Rg1、Ginsenoside Rb1 and notoginseno side R1 in dropping pills were determinded by HPLC.The assay was carried out on an ODS column

eluted with acetonitrile-water in the gradient mode.The detection wavelength was set at 203 nm

the flow rate was set at 1.0 mL·min～(-1)

and the column temperature was room temperature.Results: The major components were well identified.For ginsenoside Rg1 and ginsenoside Rb1

the linear ranges were from 0.2 μg to 1.0 μg

and for notoginsenoside R1

the linear range was from 0.1 μg to 0.5 μg

and total average recovery was 97.93%.Conclusion: The methods were feasible

reproducible and can be applied to the quality control of Xuesaitong dropping pills.

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