Studys on quality standard for Tiaojing Zimei Pills

LIU Ji-jin; XIE Yao-xuan; Xiong Ying

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Studys on quality standard for Tiaojing Zimei Pills

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- Studys on quality standard for Tiaojing Zimei Pills
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 14, Issue 5, Pages: 23-26(2008)
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- Published：2008
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LIU Ji-jin, XIE Yao-xuan, Xiong Ying. Studys on quality standard for Tiaojing Zimei Pills[J]. Chinese journal of experimental traditional medical formulae, 2008, 14(5): 23-26.
DOI：

LIU Ji-jin, XIE Yao-xuan, Xiong Ying. Studys on quality standard for Tiaojing Zimei Pills[J]. Chinese journal of experimental traditional medical formulae, 2008, 14(5): 23-26. DOI：

摘要

目的:建立调经姊妹丸的质量控制方法。方法:采用TLC法鉴别处方中青皮、丹参、大黄、莪术、肉桂;用RP-HPLC法测定该药中橙皮苷的含量。结果:在薄层色谱中能检出青皮、丹参、大黄、莪术、肉桂;橙皮苷在(10.12～253)μg·mL-1的范围内线性关系良好

r=0.9997

平均回收率为98.3%

RSD为2.7%。结论:该方法简便、准确可靠

可有效控制调经姊妹丸的质量。

Abstract

Objective:To establish a qulity stsndard for Tiaojing Zimei Pills.Methods: Pericarpium Citri Reticulatae Viride

Radix Et Rhizoma Salviae Miltirrhizae

Radix Et Rhizoma Rhei

Rhizoma Curcumae and Cortex Cinnamomi were identified by TLC

and the content of Hesperidin was determined by HPLC.Results: Pericarpium Citri Reticulatae Vidide

Radixet Et Rhizoma Salviae Miltirrhizae

Radix Et Rhizoma Rhei

Rhizoma Curcumae and Cortex Cinnamomi could be detected by TLC

Hesperidin showed a good linear relationship in the range of(10.12～253) μg·mL-1

r=(0.999 7)

The average recovery was 98.3%

and RSD was 2.7%.Conclusion: The methods are simple and accurate

and can be used for the quality control of Tiaojing Zimei Pills.

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Related Institution

The People's Hospital Affiliated to Chongqing Three Gorges Medical College

Institute of Basic Research in Clinical Medicine，China Academy of Chinese Medical Sciences

Chongqing Three Gorges Medical College

Shandong University of Traditional Chinese Medicine

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