Studies on Qualitative and Quantitative Methods of Fufangxiaojingtong Capsule

LI Lan-fang; LI Cun-man; ZHANG Qin-zeng; ZHANG Jian-xin

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Studies on Qualitative and Quantitative Methods of Fufangxiaojingtong Capsule

更新时间：2024-01-04

- Studies on Qualitative and Quantitative Methods of Fufangxiaojingtong Capsule
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 14, Issue 4, Pages: 4-5(2008)
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- Published：2008
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LI Lan-fang, LI Cun-man, ZHANG Qin-zeng, et al. Studies on Qualitative and Quantitative Methods of Fufangxiaojingtong Capsule[J]. Chinese journal of experimental traditional medical formulae, 2008, 14(4): 4-5.
DOI：

LI Lan-fang, LI Cun-man, ZHANG Qin-zeng, et al. Studies on Qualitative and Quantitative Methods of Fufangxiaojingtong Capsule[J]. Chinese journal of experimental traditional medical formulae, 2008, 14(4): 4-5. DOI：

摘要

目的:完善复方消经痛胶囊的质量标准。方法:采用薄层色谱法对复方消经痛胶囊中黄芪、白芍、香附、肉桂进行定性鉴别;并采用HLPC法对制剂中的芍药苷进行含量测定。结果:TLC鉴别专属性强;HLPC法测定出芍药苷在(0.1～2.5)μg范围内线性关系良好(r=0.9999)

平均回收率为99.5%

RSD为1.7%(n=6)。结论:所建立的定性定量方法专属性强、重复性好

可作为复方消经痛胶囊的质量控制方法。

Abstract

Objective:To Complement the quality control standards for Fufangxiaojingtong Capsule(FFXJTC).Methods: The TLC method was applied to identify Radix Astragali

Radix Paeoniae Alba

Cortex Cinnamomi and Rhizoma Cyperi;and the HPLC method was used to determine the content of paeoniflorin in FFXJTC.Results: The TLC identification methods are specific.The linear range of paeoniflorin is 0.1～2.5 μg(r=(0.999 9))

and the recovery is 99.5%

and the RSD is 1.7%(n=6).Conclusion: The qualitative and quantitative methods are specific and repeatable

which could be applied for quality control of Fufangxiaojingtong Capsule.

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Related Author

Hong-xing MA

Long-fei LIN

Yu-ling LIU

Sai FU

Jin-xin SHAO

Ji-zhong ZHU

Chuan-gui LIU

Hui LI

Related Institution

Jilin Agricultural University

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

Chengde Medical University

Jilin Huakang Pharmaceutical Co. Ltd.

The First Clinical Medical College of Guangzhou University of Chinese Medicine

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