Study on Fingerprinting of Fu Zhi San

ZHAO Jing-kun1; WANG De-sheng1; WANG Jian-xiu1; DUAN Shu-rong1; LI Wen-lan2; BAI Jing2

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Study on Fingerprinting of Fu Zhi San

更新时间：2024-09-23

- Study on Fingerprinting of Fu Zhi San
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 13, Issue 11, Pages: 4-6(2007)
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- Published：2007
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ZHAO Jing-kun1, WANG De-sheng1, WANG Jian-xiu1, et al. Study on Fingerprinting of Fu Zhi San[J]. Chinese journal of experimental traditional medical formulae, 2007, 13(11): 4-6.
DOI：

ZHAO Jing-kun1, WANG De-sheng1, WANG Jian-xiu1, et al. Study on Fingerprinting of Fu Zhi San[J]. Chinese journal of experimental traditional medical formulae, 2007, 13(11): 4-6. DOI：

摘要

目的:建立复智散反相高效液相色谱(RP-HPLC)指纹图谱的分析方法。方法:采用RP-HPLC法

线性梯度洗脱

流动相为乙腈-0.1%磷酸水溶液

体积流量1.0mL·min-1

检测波长335nm

柱温30℃。实验测定多批样品并记录指纹图谱

不同样品之间的相似度采用国家药典委员会中药色谱指纹图谱相似度评价系统研究版(2004A)计算。结果:精密度、重复性、稳定性试验中相对共有峰面积和相对保留时间的RSD均小于2%。在选定的色谱条件下确定了19个峰为复智散的指纹特征峰

自制样品平均相似度为0.996。结论:该法精密度高

重复性好

简便实用

可为复智散的指纹图谱评价提供依据。

Abstract

Objective:To establish the chromatographic fingerprints of Fu Zhi San by RP-HPLC.Methods:By RP-HPLC

acetonitrile and water including 0.1% Phosphoric acid were mobile phase with gradient elution

flow rate was 1.0 mL·min-1

the detection wavelength was 335 nm

and the temperature was 30℃.The fingerprints of different samples were compared with similarity evaluation software published by committee codex.Results:The RSD of relative peak areas and relative retention time of common peak in the test of precision

repeatability

and stability has not reached 2%

respectively.19 peaks were identified as the characteristic fingerprints.Average similarity was 0.996.Conclusion:This method is precise

practicable

well-repeated and simple.It can be used as the method to judge the quality of Fu Zhi San.

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Related Author

ZHAO Jing-kun~

王德生

王建秀

段淑荣

李文兰

白晶

Hong-xing MA

Long-fei LIN

Related Institution

1),WANG De-sheng~1,WANG Jian-xiu~1,DUAN Shu-rong~1,LI Wen-lan~2,BAI Jing~2

哈尔滨商业大学药物研究所

Jilin Agricultural University

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

Chengde Medical University

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