HPLC Determination of Andrographolide and Dehyandrographolide in Fukeqianjin Capsules

GUO Yan-rong; LU Hua

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HPLC Determination of Andrographolide and Dehyandrographolide in Fukeqianjin Capsules

更新时间：2024-01-04

- HPLC Determination of Andrographolide and Dehyandrographolide in Fukeqianjin Capsules
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 13, Issue 10, Pages: 4-5(2007)
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- Published：2007
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GUO Yan-rong, LU Hua. HPLC Determination of Andrographolide and Dehyandrographolide in Fukeqianjin Capsules[J]. Chinese journal of experimental traditional medical formulae, 2007, 13(10): 4-5.
DOI：

GUO Yan-rong, LU Hua. HPLC Determination of Andrographolide and Dehyandrographolide in Fukeqianjin Capsules[J]. Chinese journal of experimental traditional medical formulae, 2007, 13(10): 4-5. DOI：

摘要

目的:建立妇科千金胶囊中穿心莲内酯和脱水穿心莲内酯的含量测定方法。方法:以Xterra RP18色谱柱为分离柱

以甲醇-水(45∶55)为流动相

采用HPLC法测定。结果:本品中穿心莲内酯含量测定线性范围为(16～160)μg·mL-1(r=0.999 9)

平均回收率为98.4%(RSD=3.8%

n=5);脱水穿心莲内酯含量测定线性范围为(8～80)μg·mL-1(r=0.999 9)

平均回收率为98.7%(RSD=3.7%

n=5)。结论:此法操作简单、结果准确

可用于妇科千金胶囊的质量控制。

Abstract

Objective:To establish a method for the determination of Andrographolide and Dehyandrographolide in Fukeqianjin Capsules.Methods:Using the method of HPLC

the XTerra RP18 radial compression column was used with a mobile phase of methanol-water(45∶55).Results:The linear range of andrographolide was (16～160)μg·mL-1(r=0.999 9)

and the average recovery was 98.4%(RSD=3.8%

n=5);the dehydroandrographolide was(8～80)μg·mL-1(r=0.999 9)

and the average recovery was 98.7%(RSD=3.7%

n=5).Conclusion:This method was simple and feasible for the quality control of Fukeqianjin Capsules.

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Related Author

SUN Yan-rong1

WANG Yue-sheng2

LIANG Ling2

LIU Fang-ju1

YANG Fan1

DING Li1

OU Yang-xu1

Related Institution

Guangdong Province Municipal Institute of Traditional Chinese Medicine

Guangzhou University of Chinese Medicine

fong Pharmaceutical Corporation,Foshan

Guangxi University of Chinese Medicine

Guangxi Key Laboratory of Zhuang and Yao Ethnic Medicine，Guangxi University of Chinese Medicine

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