Determination of Stachydrine in Qianlietai Capsule by HPLC
|更新时间:2024-01-04
|
Determination of Stachydrine in Qianlietai Capsule by HPLC
Chinese Journal of Experimental Traditional Medical FormulaeVol. 12, Issue 9, Pages: 9-10(2006)
作者机构:
作者简介:
基金信息:
DOI:
CLC:
Published:2006
稿件说明:
移动端阅览
NING Kang-jian1, FENG Hui-ping2, HE Sheng-li2. Determination of Stachydrine in Qianlietai Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2006, 12(9): 9-10.
DOI:
NING Kang-jian1, FENG Hui-ping2, HE Sheng-li2. Determination of Stachydrine in Qianlietai Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2006, 12(9): 9-10.DOI:
Determination of Stachydrine in Qianlietai Capsule by HPLC
Objective:To develop an HPLC method for the determination of the content of Stachydrine in QLTJN.Methods:A Hypersil SCX C18 column was used as the chromatographic column.The mobile phase consisted of Potassium phosphate monobasic(0.025 mol/L
pH2.0)-Triethylamine(100∶0.25)
the flow rate was 1.0 mL/min.The UV detection wavelength was 192nm.Results:There was a good linear relationship between the concentration of Stachydrine and peak area value when the concentrations of Stachydrine was within the range of 2.8~6.5 μg(r=0.9998).The average recovery was 98^6%
RSD=0.77%(n=5).Conclusion:The method was accurate
sensitive
reproducible and may be used in the determination of Stachydrine in QLTJN.
Content Comparison of Mannose, Glucose and Narinhenin in Dendrobium officinale and Dendrobium huoshanense
Determination of Quercetin in Hawthorn Leaves by HPLC
Determination of Icariin in Ronggu Granule by HPLC
Simultaneous Determination of Evodiamine,Rutaecarpine and Evodin in Cut Crude Drug and Exact of Fructus Evodiae by High-performance Liquid Chromatography
Related Author
Ya-wen WANG
Zhi-yun LIANG
Zhen-shan XIE
Jia-hong YE
Si-jian OU
Chu-juan ZHOU
Yuan YUAN
Yue-chun HUANG
Related Institution
The First Clinical Medical College of Guangzhou University of Chinese Medicine
School of Pharmaceutical Sciences, Guangzhou University of Chinese Medicine
National Resource Center for Chinese Materia Medica, China Academy of Chinese Medical Sciences
The First Affiliated Hospital of Guangzhou University of Chinese Medicine
Level 3 Laboratory for State Administration of Traditional Chinese Medicine, Beijing Zhendong Gguangming Pharmaceutical Research Institute Co.Ltd.