HPLC法测定复方止咳宝片中吗啡的含量

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HPLC法测定复方止咳宝片中吗啡的含量

更新时间：2024-01-04

- HPLC法测定复方止咳宝片中吗啡的含量
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 10, Issue 5, Pages: 5-6(2004)
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- Published：2004
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[J]. Chinese journal of experimental traditional medical formulae, 2004, 10(5): 5-6.
DOI：

[J]. Chinese journal of experimental traditional medical formulae, 2004, 10(5): 5-6. DOI：

摘要

目的:建立复方止咳宝片中吗啡含量测定方法。方法:采用Nucleodur C18 Gravity色谱柱;流动相为甲醇-0.5%乙酸铵溶液-三乙胺(40:60:0.02);检测波长为254nm。结果:吗啡在0.5104～2.5520μg范围内具有良好的线性关系

r=0.9999

平均回收率为99.15%

RSD为1.51%。结论:该方法简便、准确、重复性好

可有效控制制剂质量。

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