Studies on Pureparation Techniques of Compound Caihutang

TONG Yan; MA Zhen-shan; WANG Lin; WANG Yuan-yu

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Studies on Pureparation Techniques of Compound Caihutang

更新时间：2024-01-04

- Studies on Pureparation Techniques of Compound Caihutang
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 8, Issue 5, Pages: 1-3(2002)
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- Published：2002
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TONG Yan, MA Zhen-shan, WANG Lin, et al. Studies on Pureparation Techniques of Compound Caihutang[J]. Chinese journal of experimental traditional medical formulae, 2002, 8(5): 1-3.
DOI：

TONG Yan, MA Zhen-shan, WANG Lin, et al. Studies on Pureparation Techniques of Compound Caihutang[J]. Chinese journal of experimental traditional medical formulae, 2002, 8(5): 1-3. DOI：

摘要

以柴胡皂苷A

芍药苷

橙皮苷

甘草酸四种指标成分的含量为指标

考察复方柴胡汤大孔吸附树脂精制工艺。结果选用1倍(生药)量S型大孔树脂

以1倍量水洗

4倍(生药量)70%乙醇洗脱树脂为最佳工艺

大孔树脂反复使用40次

干膏率、橙皮苷及芍药苷含量均无下降趋势。

Abstract

The purification conditions by absorption resins were optimized by content determination of saikosaponin A

paeoniforin

hesperidin and glycyrrhizic acid.S type synthetic absorption resin was selected.The optimal purification conditions were:specific input sample amount(ratio of weight of medical raw material to volume of resin

W/V)was one

ltime of water to elute the resin and collecting 4 times of 70% ethanol(V/W) as elution solvent.The yield and contents of paeoniforin and hesperidin of dried extract

purified by the absorption resin used repeatedly for 40 times

was not decreased compared with the new resin.

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