Quality Standard of Shentao Ruangan Capsules

JIA Jian-wei; LI Hui; ZHANG En-xin; ZHOU Dai-han; LI Yuan-bin; LAI Xiao-ping

doi:10.11653/syfj2013080063

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Quality Standard of Shentao Ruangan Capsules

更新时间：2024-01-04

- Quality Standard of Shentao Ruangan Capsules
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 8, Pages: 63-65(2013)
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- DOI：10.11653/syfj2013080063
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- Published：2013
- 稿件说明：
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JIA Jian-wei, LI Hui, ZHANG En-xin, et al. Quality Standard of Shentao Ruangan Capsules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(8): 63-65.
DOI：

JIA Jian-wei, LI Hui, ZHANG En-xin, et al. Quality Standard of Shentao Ruangan Capsules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(8): 63-65. DOI： 10.11653/syfj2013080063.

摘要

目的: 建立参桃软肝胶囊的质量控制标准。方法: 采用TLC对该制剂中生晒参、当归、丹参、大黄进行定性鉴别

采用HPLC测定人参皂苷Rb1的含量

色谱条件为以乙腈-水为流动相进行线性梯度洗脱

流速1.0 mL·min-1

检测波长203 nm。结果: TCL专属性强

均能检出目标物质

且斑点清晰

阴性对照无干扰。人参皂苷Rb1线性范围0.406～4.059 7 μg(r=0.999 7)

平均加样回收率100.96%

RSD 1.16%。结论: 方法简便准确、重复性好

可有效控制参桃软肝胶囊的质量。

Abstract

Objective: To establish the standard for quality control of Shentao Ruangan capsules. Method: Panax ginseng

Angelica sinensis

Salvia miltiorrhiza

Rheum officinale were identified qualitatively by TCL.The content of ginsenoside Rb1was determined by HPLC

chromatographic conditions were as follows:with acetonitrile-water as mobile phase in gradient elution

the detection wavelength of 203 nm

the flow rate of 1.0 mL·min-1. Result: TCL were reflecting a good specificity and could detect target substance with spots were clear and negative control was without interference.Ginsenoside Rb1 showed a good linearity at the range of 0.406-4.059 7 μg(r=0.999 7)

the average recovery was 100.96% with RSD 1.16%. Conclusion: This established method was simple

accurate and reproducible

which could effectively control the quality of Shentao Ruangan capsules.

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