Quality Standard of

LIU Lin-feng; GAO Bao-yi; GAO Shu-hong; XU Li-xia; LI Hiu-bo; LI JU-hua; LIU Zhen-dong; LIU Lai-zheng

doi:10.11653/syfj2013090077

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Quality Standard of

更新时间：2024-09-23

- Quality Standard of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 9, Pages: 77-79(2013)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.11653/syfj2013090077
  CLC：
- Published：2013
- 稿件说明：
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LIU Lin-feng, GAO Bao-yi, GAO Shu-hong, et al. Quality Standard of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 77-79.
DOI：

LIU Lin-feng, GAO Bao-yi, GAO Shu-hong, et al. Quality Standard of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 77-79. DOI： 10.11653/syfj2013090077.

摘要

目的: 修订和完善龙葵药材的质量标准。方法: 依据2010年版《中国药典》附录药品标准研究方法对龙葵药材进行显微、薄层鉴别

对10批龙葵药材的水分、灰分、酸不溶性灰分进行检查

并测定其有效成分含量。结果: 确定了龙葵药材的显微特征

并建立了其TLC鉴别方法;水分不得>10.0%

酸不溶性灰分不得>3.0%;澳洲茄碱进样量在1.002~20.04 μg内呈良好线性关系

澳洲茄边碱进样量在1.023~20.46 μg内呈良好线性关系。结论: 不同产地所含澳洲茄碱与澳洲茄边碱的总量差异较大

建立的方法能准确反映龙葵的内在质量

可作为龙葵药材质量标准的修订内容。

Abstract

Objective: To revise and improve quality standard of Solanum nigrum. Method: According to the research methods of pharmaceutical standard in 2010 version of 'Chinese Pharmacopoeia’ Appendix

S. nigrum was identified by TLC and microscopy.Moisture

ash and acid insoluble ash from 10 batches of S. nigrum were detected

and the content of active ingredients were determined. Result: Microscopic characteristics of S. nigrum was derermined

identification methods of TLC was established;The content of moisture could not more than 10%

acid insoluble ash could not more than 3.0%;Solasonine was linear in the range of 1.002-20.04 μg

but solamargine was linear in 1.023-20.46 μg. Conclusion: The total content of solasonine and solamargine from S. nigrum in different areas had significant difference.This established method could accurately reflect the inherent quality of S. Nigrum

which could be used as the amendments of quality standard for S. nigrum.

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Related Author

LIU Lin-feng1

GAO Bao-yi1

GAO Shu-hong1

XU Li-xia1

LI Hiu-bo1

LI JU-hua2

LIU Zhen-dong3

LIU Lai-zheng1

Related Institution

Taiyuan Institute for Food and Drug Control,Taiyan

Shanxi Pharmaceutical Occupational College,Taiyan

Shanxi Shuangren Pharmaceutical Co.Ltd

School of Life Science and Engineering,Southwest Jiaotong University

The First Affiliated Hospital Guangzhou University of Traditional Chinese Medicine

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