Correlation between Residues (SO) and Chemical Contents of Angelica Dahurica Radix in Different Sulfur-fumigated Degree

LU Xiao-lin; MA Yu-ying; ZHANG Fu-zhuo; ZONG Lu; JIANG Yun-bin

doi:10.11653/syfj2013090139

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Correlation between Residues (SO) and Chemical Contents of Angelica Dahurica Radix in Different Sulfur-fumigated Degree

更新时间：2024-09-23

- Correlation between Residues (SO) and Chemical Contents of Angelica Dahurica Radix in Different Sulfur-fumigated Degree
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 9, Pages: 139-142(2013)
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- DOI：10.11653/syfj2013090139
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- Published：2013
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LU Xiao-lin, MA Yu-ying, ZHANG Fu-zhuo, et al. Correlation between Residues (SO) and Chemical Contents of Angelica Dahurica Radix in Different Sulfur-fumigated Degree[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 139-142.
DOI：

LU Xiao-lin, MA Yu-ying, ZHANG Fu-zhuo, et al. Correlation between Residues (SO) and Chemical Contents of Angelica Dahurica Radix in Different Sulfur-fumigated Degree[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 139-142. DOI： 10.11653/syfj2013090139.

摘要

目的: 探讨经硫磺熏蒸后白芷的二氧化硫残留量与有效成分欧前胡素和氧化前胡素含量的相关性

为制订其科学合理、客观可控的二氧化硫限量标准提供科学依据。方法: 采用《中国药典》2010年版附录方法进行二氧化硫残留量的动态检测;采用课题组前期建立的HPLC对不同硫磺熏蒸程度的白芷进行欧前胡素和氧化前胡素的含量测定;采用曲线回归的方法进行二氧化硫残留量与有效成分含量的关联分析。结果: 自然晒干的白芷样品其二氧化硫残留量低于其他经过硫磺熏蒸的样品

氧化前胡素和欧前胡素均高于其他经过硫磺熏蒸的样品。随着硫磺用量和熏蒸时间的增加

二氧化硫残留量升高

氧化前胡素和欧前胡素的含量下降

且二者随着二氧化硫残留量增加而降低。结论: 初步探讨了随着硫磺熏蒸程度的增加

二氧化硫残留量、有效成分含量的变化规律

为下一步的深入研究提供参考。

Abstract

Objective: Inquiry into the correlation between residues (SO2) and the effective contents of imperatorin and oxypecedanin in Angelica Dahurica Radix after sulfur fumigated to provide scientific bases for formulating the scientific

rational

objective

controllable standards of sulfur dioxide limits. Method: To dynamic determine the residue of sulfur dioxide by appendix in 2010 version of 'Chinese Pharmacopoeia’ and the content of imperatorin & oxypeucedanin by HPLC. To correlation analyze the residue of sulfur dioxide and effective content by curve regression. Result: Residues (SO2) in samples without sulfur-fumigated is lower than sulfur-fumigated samples and imperatorin & oxypeucedanin in samples without sulfur-fumigated is higher than sulfur-fumigated samples. As the amount of sulfur and fumigating time increase

residues (SO2) increase and imperatorin & oxypeucedanin decrease. Conclusion: The experiment study the regulation of residues (SO2) and chemical contents with sulfur fumigation deepening to laid the foundation for the in-depth study.

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Related Author

LU Xiao-lin

MA Yu-ying

ZHANG Fu-zhuo

ZONG Lu

JIANG Yun-bin

Zhenzhen YIN

Yuzhi LIANG

Meng WANG

Related Institution

School of Pharmacy,Chengdu University of Traditional Chinese Medicine, State Key Laboratory Breeding Base of Systematic Research,Development and Utilization of Chinese Medicine Resources

School of Pharmacy，Nanjing University of Chinese Medicine

Jiangsu Key Laboratory of Chinese Medicine Processing

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

Adverse Drug Reaction Monitoring Center, Zhenjiang Institute for Food and Drug Control

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