Quality Standard of Compound Quchongbanjiuju Pill

Gulistan-Awuti; HE Cheng-hui; LIU Xuan-lin; XUE Gui-peng

doi:10.11653/syfj2013130094

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Quality Standard of Compound Quchongbanjiuju Pill

更新时间：2024-01-04

- Quality Standard of Compound Quchongbanjiuju Pill
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 13, Pages: 94-96(2013)
- 作者机构：
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- 基金信息：
- DOI：10.11653/syfj2013130094
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- Published：2013
- 稿件说明：
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Gulistan-Awuti, HE Cheng-hui, LIU Xuan-lin, et al. Quality Standard of Compound Quchongbanjiuju Pill[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(13): 94-96.
DOI：

Gulistan-Awuti, HE Cheng-hui, LIU Xuan-lin, et al. Quality Standard of Compound Quchongbanjiuju Pill[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(13): 94-96. DOI： 10.11653/syfj2013130094.

摘要

目的: 建立复方驱虫斑鸠菊丸的质量控制方法。方法: 采用显微鉴别法和薄层色谱法进行定性鉴别

高效液相色谱法测定样品中胡椒碱的含量。结果: 显微鉴别特征明显;薄层色谱鉴别斑点清晰

专属性强;含量测定胡椒碱浓度在5.42~43.36 mg·L-1呈良好线性关系

r=0.999 8(n=9)

平均回收率100.72%

RSD 0.56%。结论: 定性、定量方法简便、可靠、准确

可用于复方驱虫斑鸠菊丸的质量控制。

Abstract

Objective:To establish the method for quality control of Compound Quchongbanjiuju Pills. Method: Thin-layer chromatography and microscopic identification were used to identify Compound Quchongbanjiuju Pills. The content of pepper alkali was determined by HPLC. Result: Characteristic of microscopical identification was obvious. The TLC identification was highly specific and spots were clear. There was good linearity in the range of 5.42-43.36 mg·L-1of pepper alkali concentration (r=0.999 8)

and the average recovery of pepper alkali was 100.72% with RSD of 0.56%. Conclusion: The method is simple and accurate

which can be applied to the quality control of the Compound Quchongbanjiuju Pills.

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Related Institution

College of Pharmaceutical Science, Yunnan University of Traditional Chinese Medicine

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