Quality Standard of Baikejing Syrup

SUN Xiao-ling; SHI Fa

doi:10.11653/syfj2013130116

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Quality Standard of Baikejing Syrup

更新时间：2024-01-04

- Quality Standard of Baikejing Syrup
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 13, Pages: 116-118(2013)
- 作者机构：
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- DOI：10.11653/syfj2013130116
  CLC：
- Published：2013
- 稿件说明：
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SUN Xiao-ling, SHI Fa. Quality Standard of Baikejing Syrup[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(13): 116-118.
DOI：

SUN Xiao-ling, SHI Fa. Quality Standard of Baikejing Syrup[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(13): 116-118. DOI： 10.11653/syfj2013130116.

摘要

目的: 建立百咳静糖浆的质量控制标准。方法: 采用TLC对黄芩、黄柏、陈皮、麻黄进行定性分析

HPLC测定百咳静糖浆中黄芩苷含量。结果: 百咳静糖浆供试品与对照品色谱的相应位置上

显相同颜色斑点;Sinochrom ODS bp C18色谱柱(4.6 mm×250 mm

5 μm)

ODS预柱

流动相甲醇-水-磷酸(45∶55∶0.04)

检测波长315 nm

黄芩苷在0.08~0.4 μg呈良好线性关系(r=0.999 8)

平均回收率100.9%(RSD 1.7%)。结论: 该方法灵敏、准确可靠、重复性好

可用于百咳静糖浆的质量控制。

Abstract

Objective:To establish qualitative control standard of Baikejing syrup. Method: TLC was used for qualitative analysis of Scutellaria baicalensis

Phellodendron chinense

Citrus reticulata

Ephedra sinica

the content of baicalin was determined by HPLC. Result: Baikejing syrup for samples and reference substances showed the same color dot in corresponding chromatograph position;Sinochrom ODS bp C18 column (4.6 mm×250 mm

5 μm) and ODS pre-column were adopted with mobile phase of methanol-water-phosphoric acid(45∶55∶0.04)

detection wavelength was at 315 nm

baicalin showed a good linear relationship within the range of 0.08-0.4 μg(r=0.999 8)

the average recovery was 100.9% with RSD of 1.7%. Conclusion: This method was sensitive

reproducible and reliable

it could be used for quality control of Baikejing syrup.

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Related Author

WANG Hou-wei

GAO De-min

TIAN Jing-zhen

LI Xiao-ming

LUO Yu-jian

YUAN Yuan

HUANG Lu-qi

ZHANG Wei-hua

Related Institution

Department of Pharmacy,First Affiliated Hospital of PLA General Hospital

School of Traditional Chinese Medicine,Capital Medical University

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

College Pharmacy of Xinjiang Medical University

Shandong University of Traditional Chinese Medicine

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