Thermal Stability Investigation of -Cyclodextrin Inclusion Complex of Volatile Oil from Xiaoyu Anshen Capsules

LI Qing; SONG Guo-hong; QIN Wei-han; JIANG Yu; QIN Jian

doi:10.11653/syfj2013140017

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Thermal Stability Investigation of -Cyclodextrin Inclusion Complex of Volatile Oil from Xiaoyu Anshen Capsules

更新时间：2024-01-04

- Thermal Stability Investigation of -Cyclodextrin Inclusion Complex of Volatile Oil from Xiaoyu Anshen Capsules
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 14, Pages: 17-19(2013)
- 作者机构：
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- DOI：10.11653/syfj2013140017
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- Published：2013
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LI Qing, SONG Guo-hong, QIN Wei-han, et al. Thermal Stability Investigation of -Cyclodextrin Inclusion Complex of Volatile Oil from Xiaoyu Anshen Capsules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 17-19.
DOI：

LI Qing, SONG Guo-hong, QIN Wei-han, et al. Thermal Stability Investigation of -Cyclodextrin Inclusion Complex of Volatile Oil from Xiaoyu Anshen Capsules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 17-19. DOI： 10.11653/syfj2013140017.

摘要

目的: 考察消郁安神胶囊中挥发油β-环糊精包合物的热稳定性。方法: 采用GC-MS测定挥发油β-环糊精包合物于不同温度下百秋李醇含量。色谱条件为HP-5毛细管色谱柱(0.25 mm×30 m

0.25 μm)

Sim模式选择离子模式

检测器电压1.5 kV。结果: 挥发油包合物于40

80℃加热4 h

百秋李醇含量未发生明显变化。结论: 消郁安神胶囊中挥发油β-环糊精包合物热稳定性良好

可用于指导该制剂成型工艺设计。

Abstract

Objective: To observe thermal stability of β-cyclodextrin inclusion complex of volatile oil from Xiaoyu Anshen capsules. Method: The content of patchouli alcohol at different temperatures from β-cyclodextrin inclusion complex of volatile oil was determined by GC-MS.Chromatographic conditions were as follows:HP-5 capillary column(0.25 mm×30 m

0.25 μm)

took selective ion mode (SIM)

voltage of detector set at 1.5 kV. Result: The content of patchouli alcohol was no significant change after inclusion complex of volatile oil heating 4 h at different temperatures (40

80℃). Conclusion: Thermal stability of β-cyclodextrin inclusion complex of volatile oil from Xiaoyu Anshen capsules was good

it could guide molding process of this preparation.

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Related Author

Hui-jie YAN

Feng-qian GUO

Xin-jian LI

Yan TONG

Jin-yu WANG

Yi-ming KONG

LU Jian-qiu

LIU Ying

Related Institution

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

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