Determination of Sodium in Extract of  by ICP-MS

WANG Xiao-yi; YE Zheng-liang; ZHANG Shun-nan; ZHOU Li-hong; FAN Ying

doi:10.11653/syfj2013140034

您当前的位置：

首页 >

文章列表页 >

Determination of Sodium in Extract of by ICP-MS

更新时间：2024-01-04

- Determination of Sodium in Extract of by ICP-MS
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 14, Pages: 34-36(2013)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.11653/syfj2013140034
  CLC：
- Published：2013
- 稿件说明：
移动端阅览
WANG Xiao-yi, YE Zheng-liang, ZHANG Shun-nan, et al. Determination of Sodium in Extract of by ICP-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 34-36.
DOI：

WANG Xiao-yi, YE Zheng-liang, ZHANG Shun-nan, et al. Determination of Sodium in Extract of by ICP-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 34-36. DOI： 10.11653/syfj2013140034.

摘要

目的: 建立测定丹参提取物中钠元素含量的方法。方法: 采用硝酸为消解体系

经微波消解丹参提取物样品

通过电感耦合等离子体质谱法(ICP-MS)测定钠元素含量

为校正响应信号的变化及消除基体效应和仪器漂移的影响

选用铬元素作为内标溶液。结果: 钠元素在0.00~10.00 mg·L-1具有良好的线性关系(r=0.999 9)

以杨树叶为工作标准物质测定回收率

平均回收率90.4%

RSD 3.8%(n=6)。结论: 该方法稳定性、重复性、精密度良好

可用于测定丹参提取物中钠元素的含量。

Abstract

Objective: To establish a method for determining the content of sodium in extract of Salvia miltiorrhiza. Method: With nitric acid as digestion system

extract of S. miltiorrhiza was digested by microwave

the content of sodium belonging to this extract was determined by inductively coupled plasma mass spectrometry(ICP-MS).In order to correction response signal changes and eliminate influence of matrix effect and instrument drift

chromium was selected as an internal standard solution. Result: Linear range of sodium was 0.00-10.00 mg·L-1(r=0.999 9)

with poplar leaves as work standards

average recovery was determined as 90.4% (RSD 3.8%

n=6). Conclusion: This method had good stability

reproducibility and precision

it could be used to determining the content of sodium in extract of S. miltiorrhiza.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Analysis on Contents of Main Constituents in Prepared Morindae Officinalis Radix，Morindae Officinalis Radix Processed with Steaming and Salt

Determination of Total Flavonoids in Gubaoxinshen Tablets by UV Spectrophotometry

Determination of Flavonoids in Fructus Aurantii Immaturus by RRLC

Determination of Total Flavonoids in Prepared Medical Herbs of Cyperi Rhizoma from Different Areas

Related Author

Yi YU

Li-ping KANG

Qing-xiu HAO

Li ZHOU

Jian YANG

Long-bo ZHU

Ming-hua HU

Fang-li MA

Related Institution

State Key Laboratory Breeding Base of Genuine Herbs，National Resource Center for Chinese Materia Medica-Infinitus （China） Joint Laboratory Herbs Quality Research，National Resource Center for Chinese Materia Medica，China Academy of Chinese Medical Sciences

Beijing CACMS-NRC Herbs Testing and Auth Entication Co.Ltd.，Beijng

Infinitus（China） Co. Ltd.

Ethnic Pharmaceutical Institute of Southwest University for Nationalities

The Third Affiliated Hospital of Luohe Medical College

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰